Procedure— Ignite a suitable crucible (for example, silica, platinum, quartz, or porcelain) at 600 ± 50 for 30 minutes, cool the crucible in a desiccator (silica gel or other suitable desiccant), and weigh it accurately. Weigh accurately ◆1 to 2 g of the substance, or◆ the amount specified in the individual monograph, in the crucible.
步骤:取一个适当的坩锅(例如,硅、铂、石英、或者瓷器),在600±50 条件下灼烧30分钟,在干燥器(硅胶或者其他适合的干燥剂)中将该坩锅冷却,并精确称重。精确称取◆1-2克该物质,或者◆在具体的各论中规定的数量,于该坩锅中。
Moisten the sample with a small amount (usually 1 mL) of sulfuric acid, then heat gently at a temperature as low as practicable until the sample is thoroughly charred. Cool; then, ◆unless otherwise directed in the individual monograph, ◆moisten the residue with a small amount (usually 1 mL) of sulfuric acid; heat gently until white fumes are no longer evolved; and ignite at 600 ± 50 , ◆unless another temperature is specified in the individual monograph, ◆ until the carbon iscompletely incinerated. Ensure that flames are not produced at any time during the procedure. Cool the crucible in a desiccator (silica gel or other suitable desiccant), weigh accurately, and calculate the percentage of residue.
用少量(通常1mL)硫酸润湿该样品,然后在尽可能低的温度下温和加热至该样品彻底炭化。放凉;然后,◆除非在具体的各论中另有规定◆,以少量(通常1mL)硫酸润湿残渣;温和加热直到白色浓烟不再析出;再于600 ± 50 条件下,◆除非各论中规定其他的温度◆,灼烧,至碳被彻底焚化。确保在此步骤中的任何时间均不得出现火焰。在干燥器(硅胶或其他适当的干燥剂)中放凉该坩锅,精确称重,并计算残渣的百分比。