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The use of microelectrodes to probe the electropolymerization mechanism of heterocyclic conducting polymers

R. John and G. G. Wallace1
Chemistry Department, University of Wollongong, P.O. Box 1144, Wollongong, N.S.W. 2500 Australia
Received 18 September 1990;  revised 13 November 1990.  Available online 14 January 2002.





Abstract

Cyclic voltammetry and potential step experiments were used to investigate the electropolymerization mechanism of pyrrole at platinum micro- and macroelectrodes. The enhanced mass transport properties of microelectrodes have been used to probe certain aspects of the mechanism, particularly with respect to the formation of soluble intermediates during polymer growth. It was found that polypyrrole growth was largely the result of the continual precipitation of oligomeric intermediates from solution rather than the sequential addition of pyrrole monomers to the polymer chain ends of the deposited polymer.


1 To whom correspondence should be addressed.


Journal of Electroanalytical Chemistry
Volume 306, Issues 1-2, 24 May 1991, Pages 157-167 

抱歉，爱莫能助。

只有摘要,没有全文,只能去图书馆

你要的全文见附件！^_^
学业有成！
The use of microelectrodes to probe the electropolymerization mechanism of heterocyclic conducting polymers

原文由 zongweixu 发表:
你要的全文见附件！^_^
学业有成！
The use of microelectrodes to probe the electropolymerization mechanism of heterocyclic conducting polymers

真是太感激了，谢谢大侠！
为了兑现我的承诺，我将给你积分。另外，版主也可以再从我的积分里给你拨20分。总之40分也是值的！
再次表示感谢。

请版主给zongweixu拨20分，并且结帖、锁定帖子。谢谢！
非常感谢zongweixu的帮助，楼主已经给您悬赏的20积分了。再次表示感谢！

原文由 quanbaogang 发表:
请版主给zongweixu拨20分，并且结帖、锁定帖子。谢谢！
非常感谢zongweixu的帮助，楼主已经给您悬赏的20积分了。再次表示感谢！

每个新手应助一篇, 我一般给10分,别的人给5分,给20分的话,如果文献数多,就不好给分了