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USP467上有
Table 5. Headspace Operating Parameters
Headspace Operating | |||
1 | 2 | 3 | |
| Equilibration temperature ( ) | 80 | 105 | 80 |
| Equilibration time (min.) | 60 | 45 | 45 |
| Transfer-line temperature ( ) | 85 | 110 | 105 |
Carrier gas: nitrogen or helium at an appropriate pressure | |||
| Pressurization time (s) | 30 | 30 | 30 |
| Injection volume (mL) | 1 | 1 | 1 |
USP467上有
Table 5. Headspace Operating Parameters
Headspace Operating | |||
1 | 2 | 3 | |
| Equilibration temperature ( ) | 80 | 105 | 80 |
| Equilibration time (min.) | 60 | 45 | 45 |
| Transfer-line temperature ( ) | 85 | 110 | 105 |
Carrier gas: nitrogen or helium at an appropriate pressure | |||
| Pressurization time (s) | 30 | 30 | 30 |
| Injection volume (mL) | 1 | 1 | 1 |
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