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主题：【资料】氧化铝化验手册

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发表于：2010/05/07 09:15:55 楼主 管理 分享 倒序浏览 只看楼主 回复 私聊

目        录



第一章 生料浆制备···················

1.1 试样的采取···························

1.1.1 铝矿石和石灰石的取样····················

1.1.2 原煤的取样·························

1.1.3 焦炭的采样·························

1.1.4 纯碱的取样·························

1.1.5 氧化铝及其氢氧化铝的取样··················

1.1.6 铝酸钠浆液的取样······················

1.2 分析试样的制备·························

1.2.1 原料的烘干·························

1.2.2 试样的破碎·························

1.2.3 样品的过筛·························

1.2.4 样品的混匀·························

1.2.5 样品的缩分·························

1.2.6 铝矿石、石灰石、焦炭及熟料的试样处理············

1.2.7 矿浆、赤泥试样处理·····················

1.2.8 生料浆试样处理·······················

1.2.9 氧化铝及氢氧化铝试样处理··················

1.2.10 铝酸钠溶液的制备·····················
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第二章 试剂的配制························

2.1 试剂浓度的表示方法·······················

2.1.1 百分浓度（%）·······················

2.1.2 体积比（V：V）·······················

2.1.3 当量浓度（N）·······················

2.1.4 摩尔浓度（M）·······················

2.1.5 滴定度（T）························

2.2 标准溶液的配制和标定······················

2.2.1 标准溶液的配制方法·····················

2.2.2 标准溶液标定的方法·····················

2.2.3 标准溶液的调整·······················

2.3 酸、碱、EDTA及硝酸锌标准溶液的配制和标定···········

2.3.1 标准碱液的配制和标定····················

2.3.2 标准酸液的配制和标定····················

2.3.3 锌标准溶液的配制······················

2.3.4 EDTA标准液的配制和标定···················

2.4 其它标准溶液的配制和标定····················

2.4.1 0.1N草酸钠标准液······················

    2.4.2 0.1N高锰酸钾标准液·····················

2.4.3 0.1N氯化钠标准液······················

2.4.4 0.1N硝酸银标准液······················

2.4.5 0.1N硫氧化铵标准液·····················

2.5 比色分析标准溶液的配制·····················

2.5.1 二氧化硅标准液的配制····················

2.5.2 三氧化二铁标准液的配制···················

2.5.3 二氧化钛标准液的配制····················

2.5.4 氧化钠、氧化钾标准液的配制·················

    2.5.5 三氧化二镓标准液······················

2.6 常用试剂的配制··························   

2.6.1 常用指示剂的配制······················

2.6.2主要常用试剂的配制·····················
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第三章 铝矿石的分析·······················

3.1 二氧化硅的测定·························

3.1.1 方法概述··························

3.1.2 试剂····························

    3.1.3 操作步骤··························

3.1.4 二氧化硅标准曲线的绘制···················

3.1.5 方法说明··························

3.2 三氧化铁的测定·························

3.2.1 方法概述··························

3.2.2 试剂····························

3.2.3 操作步骤··························

3.2.4 方法说明··························

3.3 氧化铝的测定··························

3.3.1 方法概述··························   

3.3.2 试剂····························

3.3.3 操作步骤··························

3.3.4 方法说明··························

3.4 二氧化钛的测定·························

3.4.1 方法概述··························

3.4.2 试剂····························

    3.4.3 操作步骤··························

3.4.4 二氧化钛标准曲线的绘制···················

3.4.5 方法说明··························
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3.5 氧化钙的测定··························

3.5.1 方法概述··························

3.5.2 试剂····························

3.5.3 操作步骤··························

3.5.4 方法说明··························

3.6 氧化钠、氧化钾的测定······················

3.6.1 方法概述··························

3.6.2 试剂····························

3.6.3 操作步骤··························

3.6.4 标准曲线的绘制·······················

3.7 三氧化硫的测定·························

3.7.1 方法概述··························

3.7.2 试剂····························

3.7.3 操作步骤··························

3.8 氧化镓的测定··························

    3.8.1 方法概述··························

    3.8.2 试剂····························

3.8.3 操作步骤··························

3.8.4 镓的标准曲线的绘制·····················

3.9 灼减的测定···························

    3.9.1 方法概述··························

3.9.2 操作步骤··························
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第四章 石灰石、石灰极混矿的分析···············

4.1 二氧化硅、三氧化二铁、氧化铝的测定···············

4.2 石灰中氧化钙和氧化镁的连续测定·················

4.2.1 方法概述··························

    4.2.2 试剂····························

4.2.3 操作步骤··························

4.3 石灰中氧化钙的快速测定·····················

4.3.1 方法概述··························

4.3.2 试剂····························

4.3.3 操作步骤··························

4.4 石灰中有效氧化钙的测定····················· 

4.4.1 方法概述··························

4.4.2 试剂····························

4.4.3 操作步骤   
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第五章 生料浆的分析·······················

5.1 水分的测定···························

    5.1.1 方法概述··························

5.1.2 操作步骤··························

    5.1.3 比重-水分-固体含量对照表的绘制···············

5.2 细度的测定···························

5.3 成分分析用样品的制备······················

5.4 二氧化硅及三氧化二铁的测定···················

5.5 氧化铝的测定··························

5.5.1 方法概述··························

5.5.2 试剂····························

    5.5.3 操作步骤··························

5.6 氧化钙、氧化钠的测定······················

5.6.1 方法概述··························

    5.6.2 试剂····························

5.6.3 操作步骤··························

5.6.4 方法说明··························

5.7 固定碳的测定··························

5.7.1 方法概述··························

5.7.2 仪器装置··························

    5.7.3 试剂····························   

    5.7.4 操作步骤··························
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第六章 熟料、矿浆、赤泥和硅渣的分析············

6.1 二氧化硅、三氧化二铁、氧化铝及二氧化钛的测定·········

6.2 氧化钙和氧化镁合量的测定····················

6.2.1 方法概述··························

6.2.2 试剂····························

    6.2.3 操作步骤··························

6.2.4 方法说明··························

6.3 氧化钠和氧化钾的测定······················

6.3.1 硫酸盐重量法························

    6.3.1.1 方法概述·························

    6.3.1.2 试剂···························

6.3.1.3 操作步骤·························

    6.3.2 火焰光度法·························

6.3.2.1 方法概述·························

6.3.2.2 试剂···························

    6.3.2.3 操作步骤·························

6.3.2.4 标准曲线的绘制······················

6.3.2.5 方法说明·························
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6.4 硫酸钠的测定··························

    6.4.1 硫酸钡重量法························

6.4.1.1方法概述·························

    6.4.1.2试剂···························

6.4.1.3操作步骤·························

6.4.1.4方法说明·························

    6.4.2 离子交换法·························

6.4.2.1方法概述·························

6.4.2.2试剂···························

6.4.2.3操作步骤·························

6.4.2.4树脂的处理及再生·····················

6.4.2.5方法说明·························

6.5 熟料标准溶出率的测定······················

    6.5.1 方法概述··························

6.5.2 操作步骤··························

6.5.3 方法说明··························

6.6 熟料及烧结赤泥中二价硫（S2-）的测定···············

6.6.1 方法概述··························

6.6.2 试剂····························

6.6.3 操作步骤   
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第七章 铝酸钠浆液的分析····················

7.1 液固比的测定··························

7.1.1 烘干称量法·························

    7.1.2 比重法···························

7.1.2.1操作步骤·························

7.1.2.2方法说明·························

7.2 固体含量的测定·························

7.2.1 烘干称量法·························

7.2.2 沉降容积法·························

7.2.2.1操作步骤·························

7.2.2.2体积-固体含量表的制作···················

7.2.2.3方法说明·························

7.2.3 液固比换算法························

7.3 细度的测定···························

7.4 浮游物的测定··························

7.5 滤饼含水率的测定························

7.6 碱液比重的测定·························

7.7 全碱、氧化铝的测定·······················

7.7.1 方法概述··························   

    7.7.2 试剂····························

7.7.3 操作步骤··························

    7.7.4 方法说明··························

7.8 苛性碱的测定··························

7.8.1 方法概述··························

    7.8.2 试剂····························

7.8.3 操作步骤··························

7.8.4 方法说明··························

7.9 碳酸碱的测定··························

    7.9.1 方法概述··························

    7.9.2 仪器装置··························

7.9.3 试剂····························

    7.9.4 操作步骤··························
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7.10 二氧化硅测定··························

7.10.1 钼蓝比色法························

    7.10.1.1方法概述·························

7.10.1.2试剂···························

7.10.1.3操作步骤·························

7.10.1.4比色曲线绘制·······················   

    7.10.2 目视比色法························

7.10.2.1方法概述·························

    7.10.2.2试剂···························

7.10.2.3操作步骤·························

7.10.2.4二氧化硅标准级差的配制··················

7.11 三氧化二铁的测定························

7.11.1 硫氰酸盐比色法······················

7.11.1.1方法概述·························

7.11.1.2试剂···························

7.11.1.3操作步骤·························

7.11.1.4标准曲线的绘制······················

7.11.1.5方法说明·························

    7.11.2 邻二氮菲比色法······················

7.11.2.1方法概述·························

7.11.2.2试剂···························

7.11.2.3操作步骤·························

7.11.2.4标准曲线的绘制······················

7.12 硫酸根的测定··························

    7.12.1 方法概述·························

    7.12.2 试剂···························

7.12.3 操作步骤·························

7.13 氧化镓的测定··························

7.13.1 方法概述·························

7.13.2 试剂···························

7.13.3 操作步骤·························

7.14 有机物的测定··························

7.14.1 方法概述·························

7.14.2 试剂···························

7.14.3 操作步骤·························

7.15 生产用水中含碱量的测定·····················

7.15.1 方法概述·························

    7.15.2 试剂···························

7.15.3 操作步骤·························
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2010/5/7 9:21:27 10楼 管理 分享 倒序浏览 只看楼主 回复 私聊
第八章 氧化铝及氢氧化铝的分析················

8.1 二氧化硅的测定·························

    8.1.1 方法概述··························

8.1.2 试剂····························

8.1.3 操作步骤··························

8.1.4 标准曲线的绘制·······················   

8.1.5 方法说明··························

8.2 三氧化二铁的测定························

    8.2.1 方法概述··························

8.2.2 试剂····························

8.2.3 操作步骤··························

8.2.4 标准曲线的绘制·······················

8.2.5 方法说明··························

8.3 氧化钠及氧化钾的测定······················

8.3.1 火焰光度法·························

8.3.1.1方法概述·························

8.3.1.2试剂···························

8.3.1.3操作步骤·························

    8.3.1.4氧化钠及氧化钾标准曲线的制作···············

8.3.1.5方法说明·························

8.3.2 重量法···························

    8.3.2.1方法概述·························

    8.3.2.2试剂···························   

    8.3.2.3操作步骤·························

8.4 氢氧化铝附着碱的测定······················

8.4.1 方法概述··························

8.4.2 试剂····························

8.4.3 操作步骤··························

8.4.4 方法说明··························

8.5 氢氧化铝中水分的测定······················

8.5.1 方法概述··························

8.5.2 操作步骤··························

8.6 灼烧减量的测定·························

    8.6.1 方法概述··························

8.6.2 操作步骤··························

    8.6.3 方法说明 
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