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HPLC-DAD chromatograms of: a Blank rice grain sample after MSPD protocol; b Spiked rice grain sample of each one of the studied pesticide compounds. The concentrations and the elution times of the analytes were: penoxsulam (0.10 mg kg−1, 3.20 min); tricyclazole (0.10 mg kg−1, 7.01 min); 3,4-dichloroaniline (0.40 mg kg−1, 11.60 min); propanil (0.40 mg kg−1, 12.07 min), asoxystrobin (0.40 mg kg−1, 12.63 min); molinate (0.40 mg kg−1, 13.91 min); profoxydim (1.0 mg kg−1, 14.88 min); cyhalofop-butyl (0.10 mg kg−1, 16.18 min); deltamethrin (1.0 mg kg−1, 18.32 min)
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