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taoruo

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2013/3/14 9:58:13 11楼管理分享倒序浏览只看楼主回复私聊

原文由 sukiliang(sukiliang) 发表:
http://bbs.instrument.com.cn/shtml/20130217/4570465/index_2.shtml
有这个这么差么？

以下是checktune报告

Instrument Name			Instrument 1		MS Model		G6430A
Tune Date & Time			2013-02-28 15:07
Data Path			D:\MassHunter\Tune\QQQ\G6430A\Autotune_20130228_145821\atunes_20130228_150723_FAILED.TUNE.XML
Ion Source			ESI
Ionization Mode			ESI

Positive Results

*Analyzer: MS1*				*Polarity: Positive*			*Width: Unit*					X

m/z	m/z Exp	Tolerance	Delta	Result	FWHM	FWHM Exp	Tolerance	Delta	Result	Abundance	Minimum1	Result
112.3	118.1	0.1	-5.8	Adjust	11.0	0.7	0.1	10.3	Adjust	82029	#N/A	#N/A
311.7	322.1	0.1	-10.4	Adjust	4.6	0.7	0.1	3.9	Adjust	64130	0	Pass
624.3	622.0	0.1	2.3	Adjust	25.0	0.7	0.1	24.3	Adjust	2863	0	Pass
922.0	922.0	0.1	0.0	Pass	25.0	0.7	0.1	24.3	Adjust	5967	0	Pass
1222.0	1222.0	0.1	0.0	Pass	25.0	0.7	0.1	24.3	Adjust	6025	0	Pass
1822.0	1822.0	0.1	0.0	Pass	25.0	0.7	0.1	24.3	Adjust	6009	0	Pass
*Analyzer: MS2*				*Polarity: Positive*			*Width: Unit*

m/z	m/z Exp	Tolerance	Delta	Result	FWHM	FWHM Exp	Tolerance	Delta	Result	Abundance	Minimum1	Result
118.1	118.1	0.1	0.0	Pass	0.7	0.7	0.1	0.0	Pass	26791	0	Pass
321.9	322.1	0.1	-0.2	Adjust	0.8	0.7	0.1	0.1	Pass	14192	0	Pass
621.9	622.0	0.1	-0.1	Pass	0.8	0.7	0.1	0.1	Pass	10793	0	Pass
921.9	922.0	0.1	-0.1	Pass	0.8	0.7	0.1	0.1	Pass	9605	0	Pass
1221.8	1222.0	0.1	-0.2	Adjust	0.8	0.7	0.1	0.1	Pass	12761	0	Pass
1821.7	1822.0	0.1	-0.3	Adjust	0.7	0.7	0.1	0.0	Pass	8561	0	Pass
*Analyzer: MS1*				*Polarity: Positive*			*Width: Wide*

m/z	m/z Exp	Tolerance	Delta	Result	FWHM	FWHM Exp	Tolerance	Delta	Result	Abundance	Minimum1	Result
117.9	118.1	0.3	-0.2	Pass	1.3	1.2	0.6	0.1	Pass	45543	0	Pass
321.8	322.1	0.3	-0.3	Pass	1.3	1.2	0.6	0.1	Pass	21964	0	Pass
622.1	622.0	0.3	0.1	Pass	25.0	1.2	0.6	23.8	Adjust	51	0	Pass
125.0	922.0	0.3	-797.0	Adjust	25.0	1.2	0.6	23.8	Adjust	35	0	Pass
125.0	1222.0	0.3	-1097.0	Adjust	25.0	1.2	0.6	23.8	Adjust	35	0	Pass
125.0	1822.0	0.3	-1697.0	Adjust	25.0	1.2	0.6	23.8	Adjust	0	0	Pass
*Analyzer: MS2*				*Polarity: Positive*			*Width: Wide*

m/z	m/z Exp	Tolerance	Delta	Result	FWHM	FWHM Exp	Tolerance	Delta	Result	Abundance	Minimum1	Result
118.1	118.1	0.3	0.0	Pass	1.2	1.2	0.6	0.0	Pass	35065	0	Pass
322.0	322.1	0.3	-0.1	Pass	1.3	1.2	0.6	0.1	Pass	20387	0	Pass
621.9	622.0	0.3	-0.1	Pass	1.3	1.2	0.6	0.1	Pass	15866	0	Pass
921.9	922.0	0.3	-0.1	Pass	1.3	1.2	0.6	0.1	Pass	18563	0	Pass
1221.8	1222.0	0.3	-0.2	Pass	1.3	1.2	0.6	0.1	Pass	29407	0	Pass
1821.8	1822.0	0.3	-0.2	Pass	1.2	1.2	0.6	0.0	Pass	31916	0	Pass
*Analyzer: MS1*				*Polarity: Positive*			*Width: Widest*

m/z	m/z Exp	Tolerance	Delta	Result	FWHM	FWHM Exp	Tolerance	Delta	Result	Abundance	Minimum1	Result
117.8	118.1	0.5	-0.3	Pass	2.6	2.5	1.3	0.1	Pass	60454	0	Pass
321.7	322.1	0.5	-0.4	Pass	2.7	2.5	1.3	0.2	Pass	34020	0	Pass
624.9	622.0	0.5	2.9	Adjust	1.2	2.5	1.3	-1.3	Pass	459	0	Pass
125.0	922.0	0.5	-797.0	Adjust	25.0	2.5	1.3	22.5	Adjust	35	0	Pass
125.0	1222.0	0.5	-1097.0	Adjust	25.0	2.5	1.3	22.5	Adjust	35	0	Pass
1821.9	1822.0	0.5	-0.1	Pass	25.0	2.5	1.3	22.5	Adjust	35	0	Pass
*Analyzer: MS2*				*Polarity: Positive*			*Width: Widest*

m/z	m/z Exp	Tolerance	Delta	Result	FWHM	FWHM Exp	Tolerance	Delta	Result	Abundance	Minimum1	Result
118.0	118.1	0.5	-0.1	Pass	2.6	2.5	1.3	0.1	Pass	57077	0	Pass
322.0	322.1	0.5	-0.1	Pass	2.6	2.5	1.3	0.1	Pass	36102	0	Pass
621.9	622.0	0.5	-0.1	Pass	2.8	2.5	1.3	0.3	Pass	25740	0	Pass
922.0	922.0	0.5	0.0	Pass	2.5	2.5	1.3	0.0	Pass	31926	0	Pass
1222.0	1222.0	0.5	0.0	Pass	2.4	2.5	1.3	-0.1	Pass	52272	0	Pass
1821.9	1822.0	0.5	-0.1	Pass	2.5	2.5	1.3	0.0	Pass	61962	0	Pass
¹ NOTE:	1) Actual abundances depend on many factors and are instrument specific.
	To change the minimum abundance, edit the values on the "Options" sheet.


Negative Results

*Analyzer: MS1*				*Polarity: Negative*			*Width: Unit*					X

m/z	m/z Exp	Tolerance	Delta	Result	FWHM	FWHM Exp	Tolerance	Delta	Result	Abundance	Minimum1	Result
112.9	113.0	0.1	-0.1	Pass	0.8	0.7	0.1	0.1	Pass	26310	0	Pass
301.9	302.0	0.1	-0.1	Pass	0.7	0.7	0.1	0.0	Pass	118681	0	Pass
607.6	602.0	0.1	5.6	Adjust	10.5	0.7	0.1	9.8	Adjust	15897	0	Pass
607.6	1034.0	0.1	-426.4	Adjust	10.5	0.7	0.1	9.8	Adjust	0	0	Pass
607.6	1334.0	0.1	-726.4	Adjust	10.5	0.7	0.1	9.8	Adjust	0	0	Pass
607.6	1933.9	0.1	-1326.3	Adjust	10.5	0.7	0.1	9.8	Adjust	0	0	Pass
*Analyzer: MS2*				*Polarity: Negative*			*Width: Unit*

m/z	m/z Exp	Tolerance	Delta	Result	FWHM	FWHM Exp	Tolerance	Delta	Result	Abundance	Minimum1	Result
112.9	113.0	0.1	-0.1	Pass	0.7	0.7	0.1	0.0	Pass	292437	0	Pass
301.9	302.0	0.1	-0.1	Pass	0.7	0.7	0.1	0.0	Pass	128332	0	Pass
601.9	602.0	0.1	-0.1	Pass	0.7	0.7	0.1	0.0	Pass	416108	0	Pass
1033.8	1034.0	0.1	-0.2	Adjust	0.7	0.7	0.1	0.0	Pass	576498	0	Pass
1333.8	1334.0	0.1	-0.2	Adjust	0.7	0.7	0.1	0.0	Pass	962218	0	Pass
1933.7	1933.9	0.1	-0.2	Adjust	0.8	0.7	0.1	0.1	Pass	638405	0	Pass
*Analyzer: MS1*				*Polarity: Negative*			*Width: Wide*

m/z	m/z Exp	Tolerance	Delta	Result	FWHM	FWHM Exp	Tolerance	Delta	Result	Abundance	Minimum1	Result
112.9	113.0	0.3	-0.1	Pass	1.2	1.2	0.6	0.0	Pass	32043	0	Pass
301.8	302.0	0.3	-0.2	Pass	1.3	1.2	0.6	0.1	Pass	175388	0	Pass
607.4	602.0	0.3	5.4	Adjust	10.7	1.2	0.6	9.5	Adjust	17282	0	Pass
125.0	1034.0	0.3	-909.0	Adjust	25.0	1.2	0.6	23.8	Adjust	36	0	Pass
1334.0	1334.0	0.3	0.0	Pass	25.0	1.2	0.6	23.8	Adjust	39	0	Pass
1933.9	1933.9	0.3	0.0	Pass	25.0	1.2	0.6	23.8	Adjust	40	0	Pass
*Analyzer: MS2*				*Polarity: Negative*			*Width: Wide*

m/z	m/z Exp	Tolerance	Delta	Result	FWHM	FWHM Exp	Tolerance	Delta	Result	Abundance	Minimum1	Result
113.0	113.0	0.3	0.0	Pass	1.2	1.2	0.6	0.0	Pass	387095	0	Pass
301.9	302.0	0.3	-0.1	Pass	1.2	1.2	0.6	0.0	Pass	189791	0	Pass
601.8	602.0	0.3	-0.2	Pass	1.3	1.2	0.6	0.1	Pass	744957	0	Pass
1033.8	1034.0	0.3	-0.2	Pass	1.3	1.2	0.6	0.1	Pass	1392607	0	Pass
1333.7	1334.0	0.3	-0.3	Pass	1.2	1.2	0.6	0.0	Pass	2866173	0	Pass
1933.6	1933.9	0.3	-0.3	Pass	1.2	1.2	0.6	0.0	Pass	2206217	0	Pass
*Analyzer: MS1*				*Polarity: Negative*			*Width: Widest*

m/z	m/z Exp	Tolerance	Delta	Result	FWHM	FWHM Exp	Tolerance	Delta	Result	Abundance	Minimum1	Result
112.8	113.0	0.5	-0.2	Pass	2.7	2.5	1.3	0.2	Pass	39615	0	Pass
301.8	302.0	0.5	-0.2	Pass	2.8	2.5	1.3	0.3	Pass	257529	0	Pass
604.8	602.0	0.5	2.8	Adjust	1.4	2.5	1.3	-1.1	Pass	60341	0	Pass
125.0	1034.0	0.5	-909.0	Adjust	25.0	2.5	1.3	22.5	Adjust	36	0	Pass
125.0	1334.0	0.5	-1209.0	Adjust	25.0	2.5	1.3	22.5	Adjust	0	0	Pass
125.0	1933.9	0.5	-1808.9	Adjust	25.0	2.5	1.3	22.5	Adjust	0	0	Pass
*Analyzer: MS2*				*Polarity: Negative*			*Width: Widest*

m/z	m/z Exp	Tolerance	Delta	Result	FWHM	FWHM Exp	Tolerance	Delta	Result	Abundance	Minimum1	Result
112.9	113.0	0.5	-0.1	Pass	2.6	2.5	1.3	0.1	Pass	536778	0	Pass
301.9	302.0	0.5	-0.1	Pass	2.6	2.5	1.3	0.1	Pass	287462	0	Pass
601.9	602.0	0.5	-0.1	Pass	2.6	2.5	1.3	0.1	Pass	1114457	0	Pass
1033.9	1034.0	0.5	-0.1	Pass	2.5	2.5	1.3	0.0	Pass	2457502	0	Pass
1333.8	1334.0	0.5	-0.2	Pass	2.5	2.5	1.3	0.0	Pass	5538127	0	Pass
1933.8	1933.9	0.5	-0.1	Pass	2.3	2.5	1.3	-0.2	Pass	5264742	0	Pass
¹ NOTE:	1) Actual abundances depend on many factors and are instrument specific.
	To change the minimum abundance, edit the values on the "Options" sheet.

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sukiliang

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ID：sukiliang

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结帖率：

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新手级：新兵

2013/3/14 12:03:09 12楼管理分享倒序浏览只看楼主回复私聊

原文由 taoruo(taoruo) 发表:
原文由 sukiliang(sukiliang) 发表:
http://bbs.instrument.com.cn/shtml/20130217/4570465/index_2.shtml

有这个这么差么？

试一下换个调谐液，如果both不行先调谐正模式！

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