PDF#46-1043: QM=Star(+); d=Diffractometer; I=Diffractometer
Palladium, syn
Pd (Black)
Radiation=CuKa1 Lambda=1.5405981 Filter=Ge
Calibration=Internal(Si) d-Cutoff= I/Ic(RIR)=4.1
Ref= Kern, A., Eysel, W., Mineralogisch-Petrograph. Inst., Univ. Heidelberg, Germany.
ICDD Grant-in-Aid (1993)
Cubic - Powder Diffraction, Fm-3m (225) Z=4 mp=
Cell=3.8902 Pearson=cF4 (Cu)
Density(c)=12.004 Density(m)=12.02A Mwt=106.40 Vol=58.87 F(8)=615.4(.0016,8)
Ref= Ibid.

Strong Line: 2.25/X 1.95/6 1.17/6 1.38/4 0.89/4 1.12/2 0.97/1 0.87/1 0.00/1 0.00/1
NOTE: Pd (Heraeus, 99.99%).
2$GU determination based on profile fit method.
To replace 00-005-0681.
d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d
2.2458 100.0 95.0 1 1 1 3 40.118 20.059 0.2226 2.7977
1.9451 60.0 66.0 2 0 0 4 46.658 23.329 0.2571 3.2302
1.3754 42.0 65.0 2 2 0 8 68.119 34.059 0.3635 4.5684
1.1730 55.0 100.0 3 1 1 11 82.098 41.049 0.4263 5.3567
1.1230 15.0 28.0 2 2 2 12 86.617 43.308 0.4452 5.5951
0.9725 13.0 29.0 4 0 0 16 104.751 52.376 0.5141 6.4606
0.8925 40.0 96.0 3 3 1 19 119.329 59.665 0.5602 7.0402
0.8699 11.0 27.0 4 2 0 20 124.627 62.313 0.5748 7.2230

PDF#65-2867: QM=Calculated; d=Calculated; I=Calculated
Palladium
Pd
Radiation=CuKa1 Lambda=1.54060 Filter=
Calibration= d-Cutoff= I/Ic(RIR)=17.26
Ref= Calculated from NIST using POWD-12++

Cubic - (Unknown), Fm-3m (225) Z=4 mp=
Cell=3.8908 Pearson=cF4 (Cu)
Density(c)=11.996 Density(m)=12.02A Mwt=106.40 Vol=58.90 F(8)=999.9(.0001,8)
Ref= B.Coles
J. Inst. Met., 84 346 (1956)
Strong Line: 2.25/X 1.95/4 1.17/2 1.38/2 0.89/1 0.87/1 1.12/1 0.97/1 0.00/1 0.00/1
NOTE: N AL3277 6632 IB=Pd See PDF 03-05-6174.
d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d
2.2464 100.0 100.0 1 1 1 3 40.108 20.054 0.2226 2.7971
1.9454 44.9 51.9 2 0 0 4 46.650 23.325 0.2570 3.2298
1.3756 22.8 37.2 2 2 0 8 68.105 34.053 0.3635 4.5676
1.1731 23.6 45.2 3 1 1 11 82.083 41.042 0.4262 5.3560
1.1232 6.7 13.4 2 2 2 12 86.598 43.299 0.4452 5.5941
0.9727 3.2 7.4 4 0 0 16 104.727 52.363 0.5140 6.4595
0.8926 10.9 27.4 3 3 1 19 119.299 59.650 0.5602 7.0391
0.8700 10.6 27.4 4 2 0 20 124.594 62.297 0.5747 7.2220

PDF#65-6174: QM=Calculated; d=Calculated; I=Calculated
Palladium
Pd
Radiation=CuKa1 Lambda=1.54060 Filter=
Calibration= d-Cutoff= I/Ic(RIR)=16.42
Ref= Calculated from NIST using POWD-12++

Cubic - (Unknown), Fm-3m (225) Z=4 mp=
Cell=3.8874 Pearson=cF4 (Cu)
Density(c)=12.028 Density(m)=12.02A Mwt=106.40 Vol=58.75 F(8)=999.9(.0000,8)
Ref= King, H. W., Manchester, F. D.
J. Phys. F, 8 15 (1978)
Strong Line: 2.24/X 1.94/4 1.37/2 1.17/2 0.89/1 0.87/1 1.12/1 0.97/1 0.00/1 0.00/1
NOTE: L 44719 42357 0 TF was not given, B set to 1.000 for calc.
The Pd rod was process-annealed for 2hr at 367C and the heated for a few minutes to 800C to remove residual stresses.
Materials Research Corporation 20 A low temperature x ray diffraction study of Pd and some Pd-H alloys See PDF 03-065-2867 and 01-089-4897.
d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d
2.2444 100.0 100.0 1 1 1 3 40.144 20.072 0.2228 2.7995
1.9437 44.2 51.1 2 0 0 4 46.694 23.347 0.2572 3.2326
1.3744 21.0 34.3 2 2 0 8 68.174 34.087 0.3638 4.5716
1.1721 20.9 40.0 3 1 1 11 82.170 41.085 0.4266 5.3606
1.1222 5.7 11.4 2 2 2 12 86.692 43.346 0.4456 5.5990
0.9718 2.6 6.0 4 0 0 16 104.857 52.428 0.5145 6.4652
0.8918 8.5 21.4 3 3 1 19 119.471 59.735 0.5606 7.0453
0.8692 8.1 20.9 4 2 0 20 124.785 62.393 0.5752 7.2283
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