主题:【求助】NMR 测试参数意义

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liangyuegan0123
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是个门外汉, 刚做了13CNMR, 测试报告中英文参数不太清楚,请专家详细点解释,谢谢
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ZZF
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400MHz谱仪,13C共振频率是100.6MHz.
转子7mm,实验脉冲序列是:cp(交叉极化)
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Utopia
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帮你直接列出参数,请高手解释:

Name   
EXPNO   
PROCNO   
     
Acquisition Parameters   
Date_   
Time   
INSTRUM   
PROBHD   
PULPROG   
TD   
SOLVENT   
NS   
DS   
SWH   
FIDRES   
AQ   
RG   
DW   
DE   
TE   
D1   
ZGOPTINS   
     
=======CHANNEL f1=========   
NUC1   
P1   
PL1   
SF01   
     
Processing Parameters   
SI   
SF   
WDW   
SSB   
LB   
GB   
PC   
     
1D NMR Plot Parameters   
CX   
CY   
F1P   
F1   
F2P   
F2   
PPMCM   
HZCM   
 
fourhappy
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NAME: experiment name
EXPNO: experiment number
PROCNO: product number
Date-Time:the date and time of measurement
INSTRUM:spect
PROBHD:probhead type
PULPROG:pulse programme
TD:time domain size
SOLVENT:
NS:numbers of scan
DS:dummy scan
SWH(Hz):Sweep width in Hz
FIDRES:
AQ:acquisition time
RG:receiver gain
DW:dwell time
DE:pre-scan-delay
TE:temperature
D1:relaxation delay, 1-5*T1
TD0: dimension of accumulation loop
----------------f1channel---------------
Nuc1:Nucleus for channel 1 ----1H
P1:F1 channel- 90 degree high power pulse
PL1:F1 channel- power level for pulse (default)
SFO1:Frequency of observe channel
SI:Size of real spectrum
SF:Spectrometer frequency
WDW:window functions for trf, xfb….
SSB:Sine belt shift SSB(0,1,2,…)
LB:Line broadening for em
GB:Gaussian max, position for gm, 0<GB<1
PCPeak detection sensitivity for pp
该帖子作者被版主 kcq19972积分, 2经验,加分理由:积极回答
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2010/7/19 10:51:02 Last edit by fourhappy
fourhappy
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it is for H above.

C谱各参数意义
NAME: experiment name
EXPNO: experiment number
PROCNO: product number
Date-Time:the date and time of measurement
INSTRUM:spect
PROBHD:probhead type
PULPROG:pulse programme
TD:time domain size
SOLVENT:
NS:numbers of scan
DS:dummy scan
SWH(Hz):Sweep width in Hz
FIDRES:
AQ:acquisition time
RG:receiver gain
DW:dwell time
DE:pre-scan-delay
TE:temperature
D1:relaxation delay, 1-5*T1
D11:
TD0: dimension of accumulation loop
----------------channel f1---------------
Nuc1:Nucleus for channel 1 ----13C
P1:F1 channel- 90 degree high power pulse
PL1:F1 channel- power level for pulse (default)
SFO1:Frequency of observe channel
------------ channel f2---------------
CPDPRG2:
NUC2: Nucleus for channel 1 ----1H
PCPD2:
PL2: F2 channel- power level for pulse
PL12:
PL2W: F2 channel- power level for pulse
SFO2: Frequency of decouple channel
SI:Size of real spectrum
SF:Spectrometer frequency
WDW:window functions for trf, xfb….
SSB:Sine belt shift SSB(0,1,2,…)
LB:Line broadening for em
GB:Gaussian max, position for gm, 0<GB<1
PC:Peak detection sensitivity for pp
liangyuegan0123
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lipi0929
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