When operating a scanning force microscope in a dynamic mode the oscillation of the cantilever is influenced by non-linear interaction forces between the probing tip and the surface. In principle the instantaneous forces exerted on the sample while scanning the surface can be either repulsive or attractive. Experimental findings and corresponding computer simulations of the tapping mode show that by choosing appropriate system parameters the scanning force microscope can continuously be operated in the regime of net-attractive interaction forces. Thereby the risk of modifying the sample surface by the probing tip is minimized. However, in most cases the range in which the system parameters have to be adjusted is rather narrow and therefore a stable operation of the scanning force microscope in this interaction regime is difficult to achieve.
With the help of the Q-Control module it is possible to reduce the damping of the dynamic system, i.e. to increase the effective quality factor of the oscillating cantilever and thereby to enlarge the regime of net-attractive interaction forces. This method allows the user to minimize the forces exerted by the probing tip on the sample surface. Therefore by applying Q-Control delicate and highly sensitive surface structures that could not be scanned with a standard scanning force microscope can now be characterized with high resolution. Typical resonance curve of a free oscillating silicon cantilever in air. By applying Q-Control the effective quality factor was increased from about 450 to almost 20000. The high quality factor implicates a steep slope of the phase signal.
In a liquid medium the oscillation of a cantilever is strongly affected by hydrodynamic damping. This leads to quality factors in the single digit range and a loss in force sensitivity. The Q-Control technique as a countermeasure allows increasing the effective quality factor up to three orders of magnitude in liquids
When operating a scanning force microscope in a dynamic mode the oscillation of the cantilever is influenced by non-linear interaction forces between the probing tip and the surface. In principle the instantaneous forces exerted on the sample while scanning the surface can be either repulsive or attractive. Experimental findings and corresponding computer simulations of the tapping mode show that by choosing appropriate system parameters the scanning force microscope can continuously be operated in the regime of net-attractive interaction forces. Thereby the risk of modifying the sample surface by the probing tip is minimized. However, in most cases the range in which the system parameters have to be adjusted is rather narrow and therefore a stable operation of the scanning force microscope in this interaction regime is difficult to achieve.
With the help of the Q-Control module it is possible to reduce the damping of the dynamic system, i.e. to increase the effective quality factor of the oscillating cantilever and thereby to enlarge the regime of net-attractive interaction forces. This method allows the user to minimize the forces exerted by the probing tip on the sample surface. Therefore by applying Q-Control delicate and highly sensitive surface structures that could not be scanned with a standard scanning force microscope can now be characterized with high resolution. Typical resonance curve of a free oscillating silicon cantilever in air. By applying Q-Control the effective quality factor was increased from about 450 to almost 20000. The high quality factor implicates a steep slope of the phase signal.
In a liquid medium the oscillation of a cantilever is strongly affected by hydrodynamic damping. This leads to quality factors in the single digit range and a loss in force sensitivity. The Q-Control technique as a countermeasure allows increasing the effective quality factor up to three orders of magnitude in liquids
我的社区
签到
赛默飞实验室产品焕新计划有奖调研！
【七月征文】不一YOUNG实验“猿”
报名开启：ICS2024第十三届光谱网络会议！
推荐收藏！盘点中药材及饮片检测解决方案
