主题：请问有没有多维（三、四维）NMR在聚合物方面应用的文献？？

好像在03年的macromolecules中有一篇，是杜邦公司研究人员的文章

wo我觉得比较少，面太窄了

这方面的文献很多的,下面给出一些供参考.

"Characterization of Polymer Chain Ends of Polybutadiene Using 1H/13C/119 Sn Triple Resonance 3D-NMR," Liu, W.; Saito, T.; Li, L.; Rinaldi, P.L.; Hirst, R.; Halasa, A.F.; and Visintainer, J., Macromolecules, 2000, 33, 2364.

"1H/13C/119Sn Triple Resonance 3D-NMR of Tin-Containing Polybutadiene," Liu, W.; Halasa, A.F.; Visintainer, J.; Hirst, R.; and Rinaldi, P.L., Polymer Preprints, 2000, 41(1), 26.

NMR 3D Analysis Photopolymerization

by N. Fatkullin et al
This volume presents critical reviews of the present and future trends in polymer and biopolymer science including chemistry, physical chemistry, physics and materials science.

NMR 3D Analysis Photopolymerization's objective is to outline the basic theories and models of linear polymer chain dynamics and to demonstrate the potential of NMR (nuclear magnetic resonance) techniques for probing the characteristics of molecular motions in such systems. From the methodological point of view, it mainly focuses on field-cycling NMR relaxometry and field-gradient NMR diffusometry, but also makes some references to transverse relaxation and the residual dipolar interaction occuring in entangled polymer systems.

It is addressed to all scientists at universities and in industry who wish to keep abreast of advances in the topics covered.

Contents

Polymer Chain Dynamics and NMR
Introduction
NMR Methods
Modeling of Chain Dynamics and Predictions for NMR Measurands
Experimental Studies of Bulk Melts, Networks and Concentrated Solutions
Chain Dynamics in Pores ("Artificial Tubes")

Emerging Technologies for the 3D Analysis of Polymer Structures
Introduction
3D Microscopy
Digital Image Analysis of 3D Structures
Time Evolution of Bicontinuous Structure in Spinodal Interface of a Binary Polymer Mixture
Direct Measurement of Interfacial Curvature Distributions in a Bicontinuous Block Copolymer Nanostructure
Geometrical Similarity/Difference Between Polymer Blend and Block Copolymer Structures

Two-Photon Photopolymerization and 3D Lithographic Microfabrication
Introduction
General Stereolithography Using Femtosecond Lasers
Fundamentals of Stereolithography using Two-Photon Photopolymerization
Advanced Techniques in Two-Photon Micro-Nanofabrication
Applications
Future Prognosis
Author Index
Subject Index

The 2D and 3D NMR experiments generate huge data sets, Rinaldi noted. The lab
has a network with primarily Windows NT, ... "We do a lot of polymer analysis,"
Rinaldi noted. And while there are small compilations of NMR resonances

http://www.acdlabs.com/publish/sca.html

It is a package for computer-assisted assignment of 2D, 3D, and 4D NMR. spectra of
proteins and nucleic acids, which includes tools for ... Polymer Builder. is used
to construct models of polymer chains from monomers

3D Methods. 3.4.1 Homonuclear 3D Experiments. 3.4.2 Assignment-oriented
Heteronuclear 3D NMR. 3.4.3 Heteronuclear 3D with 15N/13C-labeled ... 10.4 Polymer
Segment End-Structure Determination by Long-Range Correlation Experiments

Two-Dimensional NMR Spectroscopy: Applications for Chemists and Biochemists, Second Edition, Fully Updated and Expanded to Include Multidimensional Work
W. R. Croasmun (Editor), Robert M. K. Carlson (Editor)
ISBN: 0-471-18593-0
Hardcover
980 pages
August 1994

谢谢celan老师  真不少啊 我忘了用google搜了，输入Multidimensional和polymer 唰一下就一千多条 真有的忙了

其实我想找一些固体核磁多维（三、四维）谱在固态高聚物方面的应用，还是比较困难啊，现在找到的大多是用液体多维NMR研究聚合物

学到了好多东西啊