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chengjingbao
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今天继续第9章第6段,仪器常规维护。
9.6 Routine check-up常规检查
The analyzer does not need a lot of supervision. But for accurate measurements you must be sure that:
分析仪不需要过多的管理。但是仪器的精密测量度你一定有把握做到:
1. Carrier flow is as per the value specified for your configuration. To check the carrier flow, put the injection mode in manual. Go back in «RUN» menu and watch the value. It is normal to have carrier flow deviation during a cycle. Between and before an injection the carrier flow must be correct.
载气流量按照你的仪器配置的设定值。检查载气流量,将进样模式改为手动。返回《运行》菜单并检查数值。通过这个标准,检查载气在常规状态下和分析周期期间两者之间的背离情况。在这之前,载气流量必须正确选择好。
2. From time to time, verify the oven temperature in the diagnostic menu. It must be constant and at the value specified in the configuration section in the back cover.
有时,在诊断菜单里查证柱温。这必须是一个恒定温度且背面配置章节里设定值。
3. The sample flow must be at the same value of the previous calibration procedure. This is to make sure you have the same sample volume injected. The default value of 75 sccm is OK.
样品流量必须与校验时的流量值相一致。必须确定你进的是同等体积的样品量。默认值是75就可以啦。
4. Clean cabinet fan’s filter periodically. This is very important, high internal temperature will eventually cause problems.
定期清洁你的风扇过滤网,这非常重要,内部温度高将导致产生问题信息。
该帖子作者被版主 何当奇3积分, 2经验,加分理由:有效求助
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何当奇
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The analyzer does not need a lot of supervision. But for accurate measurements you must be sure that:
分析仪不需要过多的管理。但是仪器的精密测量度你一定有把握做到:
分析仪所需监管不多,但要做到精确测定,需确保以下(操作)
youjian000
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It is normal to have carrier flow deviation during a cycle.
在分析周期期间,载气流量有偏差(微小的变化)是正常的.
该帖子作者被版主 redanqi3积分, 2经验,加分理由:应助
youjian000
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Between and before an injection the carrier flow must be correct.
在进样前以及进样之间,必须校正载气流量.
youjian000
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It must be constant and at the value specified in the configuration section in the back cover.
问一下程兄:仪器的后盖是否有一个参数配置区域?
何当奇
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1. Carrier flow is as per the value specified for your configuration. To check the carrier flow, put the injection mode in manual. Go back in «RUN» menu and watch the value. It is normal to have carrier flow deviation during a cycle. Between and before an injection the carrier flow must be correct.
载气流量按照你的仪器配置的设定值。检查载气流量,将进样模式改为手动。返回《运行》菜单并检查数值。通过这个标准,检查载气在常规状态下和分析周期期间两者之间的背离情况。在这之前,载气流量必须正确选择好。
载气流量以(分析仪)配置值而定。检查载气流量时,将进样模式设为手动。正常情况下,一个循环(或者周期)间,会有载气流偏差。进样前和进样间必须校正载气流。
何当奇
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2. From time to time, verify the oven temperature in the diagnostic menu. It must be constant and at the value specified in the configuration section in the back cover.
有时,在诊断菜单里查证柱温。这必须是一个恒定温度且背面配置章节里设定值。
不时 (经常地)在诊断菜单里查证炉温。此炉温必须恒定且在背盖设置部分所设定值中。
第二句有点糊涂。
何当奇
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3. The sample flow must be at the same value of the previous calibration procedure. This is to make sure you have the same sample volume injected. The default value of 75 sccm is OK.
样品流量必须与校验时的流量值相一致。必须确定你进的是同等体积的样品量。默认值是75就可以啦 (即可)。

何当奇
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4. Clean cabinet fan’s filter periodically. This is very important, high internal temperature will eventually cause problems.
定期清洁你的风扇过滤网,这非常重要,内部温度高将导致产生问题信息。
定期清洁橱柜风扇过滤网。这点非常重要,内部高温将最终引发问题。
chengjingbao
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原文由 youjian000 发表:
It must be constant and at the value specified in the configuration section in the back cover.
问一下程兄:仪器的后盖是否有一个参数配置区域?

没有,但有一个外接输出端口,用于外接计算机,可对它进行参数配置。仪器内部配置好的参数,也可进行下载,若参数紊乱,上传计算机内保存的参数即可。
chengjingbao
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原文由 youjian000 发表:
Between and before an injection the carrier flow must be correct.
在进样前以及进样之间,必须校正载气流量.


这一点我的观点是,在进样前以及进样之间,必须确保载气流量的稳定must be correct。
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