Simultaneous Determination of Residues of Approximately 100 Pesticides and Metabolites in Fruit and Vegetables by LC/MS/MS(
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Experimental
Extraction and cleanup procedures are described in Figure 1. Using the readyfor- use method files on the CD ROM in combination with API 2000, API 3000, and API 4000 LC/MS/MS Systems following pesticides and their metabolites can be identified and quantified: 3,4,5-trimethacarb, 3-hydroxycarbofuron, 5-hydroxyclethodimsulfone, 5-hydroxythiabendazole, acephate, aldicarb, aldicarbsulfoxide, aldoxycarb, amidosulfuron, atrazine, azoxystrobin, bendiocarb, bensulfuronmethyl, butocarboxim, butocarboxim-sulfoxide, butoxycarboxim, carbaryl, carbendazim, carbofuran, chlorsulfuron, cinosulfuron, clethodim, clethodimiminsulfone, clethodimiminsulfoxide, clethodimsulfone, clethodimsulfoxide, cyprodinil, daminozid, demeton-S-methyl, demeton-S-methylsulfone, desmedipham, desmethylformamidopirimicarb, desmethylpirimicarb, dimethoate, diuron, ethiofencarb, ethiofencarbsulfone, ethiofencarbsulfoxide, fenhexamid, fenoxycarb, fenpropimorph, flazasulfuron,
florasulam, fluazifoppbutyl, flufenoxuron, fosthiazate, furathiocarb, haloxyfopethoxyethyl, haloxyfopethyl, imazalil, imidacloprid, indoxacarb, iodosulfuronmethyl, iprovalicarb, isoproturon, linuron, metalaxyl, metamitron, methamidophos, methiocarb, methomyl, metolachlor, metsulfuronmethyl, monocrotophos, nicosulfuron, omethoate, oxamyl, oxydemetonmethyl, phenmedipham, pirimicarb, primisulfuronmethyl, promecarb, propamocarb, propoxur, prosulfuron, pymetrozin, pyridate, pyridatmetabolite, pyrimethanil, quinmerac, quizalofopethyl, rimsulfuron, spiroxamine, tebuconazole, tebufenozid, thiabendazol, thiacloprid, thifensulfuronmethyl, thiodicarb, thiofanox, thiofanoxsulfone, thiofanoxsulfoxide, thiophanatmethyl, triasulfuron, tribenuronmethyl, triflusulfuronmethyl and vamidothion (Figure 2).