主题:【求助】ATR红外的锗晶体污染可以用什么清洗

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happyalife
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原文由 sophaloki(sophaloki) 发表:
谢谢大家的帮助,我的红外是尼高力的,我用擦镜纸使劲的弄都弄不掉,也不敢用溶剂洗,怕影响光路。以前也出现过弄脏了,后来也不知道那个东西怎么就没了的!


太神奇了,这次就不能让它莫名其妙的就没了么
sophaloki
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原文由 happyalife(happyalife) 发表:
原文由 sophaloki(sophaloki) 发表:
谢谢大家的帮助,我的红外是尼高力的,我用擦镜纸使劲的弄都弄不掉,也不敢用溶剂洗,怕影响光路。以前也出现过弄脏了,后来也不知道那个东西怎么就没了的!


太神奇了,这次就不能让它莫名其妙的就没了么


呵呵,还真的没了,我就是每次做红外的时候就会用擦镜纸使劲擦,没想到擦了几回,居然被我擦掉了。目前还没有发现对测试有什么影响呢。说真的,我自己真的不敢蘸酒精之内的清洗!
ghcily
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呵呵,估计酒精对晶体没有影响吧!用酒精估计是可以的!
chemhehe
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这方面我是专家:)
一般情况下,滴几滴氧化铝悬浮液到打磨布(polishing cloth)上,再在上面加一点水,将atr晶体在上面磨一磨,然后用水冲干净就行了。
oscarjxc
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怎样清洁红外窗片和晶体

要清理的光学元件,如KBr、CaF2、BaF2、ZnSe窗片或晶体等,一般可用棉签蘸合适的溶剂多次涂抹来清洁元件表面。在一般情况下,清洗盐类(如溴化钾,氯化钠)应避免使用水或含水的溶剂。非盐材料可以用清水清洗。一般用于清洁的有机溶剂是无水乙醇,丙酮,甲基乙基酮(MEK)。这些溶剂在使用前,应确认是无水的。蘸过溶剂的棉签应轻轻在窗片或晶体表面滑过或滚过,以免滑伤表面。另一种方法是使用超声波清洗浴缸。光学元件放置在培养皿中或软材料(如聚四氟乙烯)之上,尽量避免光学元件与其他材料接触。用适当的溶剂或清洁剂覆盖表面。约清洗0.5小时。使用低功耗等离子清洗机,也可以实现非接触式光学元件的清洗。确认窗口或ATR晶体是否清洗干净,常见的方法就是在仪器上来做一个单光束光谱,并与和以前的背景光谱作比对,不存在异常的高吸收峰,就说明清洗干净了。
    对不太严重的沾污或划伤的元件,还可以用专用清洁包来抛光处理。
 
To clean optical elements, most people use cotton-tipped applicators with a suitable solvent.. In general, avoid the use of water or solvents with water when cleaning salts (e.g., KBr, NaCl). Many non-salt materials can be cleaned with water. Many materials in general can be cleaned with organic solvents such as alcohol, acetone, and methyl ethyl ketone (MEK). MEK is a particularly good solvent for cleaning optical materials, because of its high volatility.
Another method of cleaning windows and ATR elements is to use an ultrasonic cleaning bath. With this equipment, cleaning is accomplished without abrasion. (Such cleaning baths are available through the major laboratory equipment suppliers.) The optical elements are placed in a tray or shallow bottle, on top of a soft material (e.g., PTFE), so that no two elements are touching. The elements are then covered with a suitable solvent and the cleaner turned on for approximately one hour. Non-contact cleaning of optical elements may also be accomplished using a low power plasma cleaner.
One common method to verify that the window or ATR element is clean is to run a single beam spectrum and look for unusual peaks that were not present in previous background spectra using the same equipment. Obviously, no amount of cleaning will restore an optical element which has been scratched, chipped, or broken. Minor defects can be corrected using the Optical Polishing Kit.
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2012/5/23 18:05:08 Last edit by tangtang
fyrebecca
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我所有的ATR晶体基本都是棉花蘸酒精完成的
金刚石和锗的话耐磨耐压,使劲擦也没关系
ZnSe的晶体需要比较小心,轻轻擦,多蘸点,保持整个棉花都是湿润状态,上面有人提到的用打磨布肯定是不行的,ZnSe非常不耐刮擦,很容易就划伤了
tangtang
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