毛细管
气相色谱分析方法的可预测性转换在快速
gc 中的应用
Abstract: 毛细管
气相色谱(
gc) 运行分析时间常常是决定样品总分析时间的重要因素。快速
gc 法通过减少分析时间大大提高了实验室工作效率。然而,将已建立的毛细管
gc 分析方法转换为快速
gc 分析方法是一项艰巨的任务。 Agilent
gc 方法转换软件是一个免费软件程序,它可合理和可预测地把传统毛细管
气相色谱分析方法转换为快速
gc 方法。这一转换程序保留了每种化合物的流出顺序,无须再对每一个峰进行认定。新方法的验证非常容易。这一方法转化软件可以立即对温度、流速进行计算以适应各种要求,包括保留时间锁定,最高理论柱效和缩短分析时间。本应用研究论述了根据传统
gc 方法选择快速
gc 方法时需要注意的事项,描述了Agilent
gc 方法转换软件,并验证了转换方法可以快速分析溶剂、苯乙烯单体、重整汽油、烃类排放物、半挥发性混合物和化工中间体。 The time required for capillary gas chromatography (
gc) runs is often the major factor in sample turnaround time. Fast
gc can significantly improve laboratory productivity by decreasing analysis time. However, converting established capillary
gc methods to fast
gc can be a daunting task. The Agilent
gc method translation software is a freeware program that logically and predictably translates traditional capillary
gc methods. The translation program preserves the elution order for each compound, so that identification of each peak does not have to be repeated. Validation for the new method is made easier. The method translation software will instantly calculate temperature and flow conditions to meet various requirements including retention time locking, best theoretical efficiency, and decreased time. This application note discusses considerations involved in choosing fast
gc over conventional
gc, describes the Agilent
gc method translation software, and demonstrates translating methods for faster analysis of solvents, styrene monomers, reformate gasoline, hydrocarbon emissions, semivolatile mixtures, and a chemical process intermediate.
Keywords: capillary gas chromatography (
gc), Fast
gc,
gc,
gc method translation, method translation software 毛细管
气相色谱(
gc),快速
气相色谱,
气相色谱,
气相色谱方法转化,方法转换软件