今天收到一份bruker衍射仪器测试的数据,看了一下,没太看懂,发现它的最强峰不到20,并且背景都是不连续的,估计是保存或者我转化时出了问题。bruker和panalytical的仪器设置应该差不多,我估计。
参数如下:
_FILEVERSION=2
_SITE='enter the name of your site'
_USER='enter your name'
_GONIOMETER_CODE=2580
; D8 Theta/2Theta; High Temperature
_SAMPLE_CHANGER_CODE=0
_ATTACHMENTS_CODE=0
_GONIOMETER_RADIUS=217.500000
_FIXED_DIVSLIT=1.000000
_FIXED_SAMPLESLIT=0.000000
_FIXED_DETSLIT=12.060000
_MONOCHROMATOR=0
; None
_THIN_FILM='N'
_BETA_FILTER='N'
_FIXED_ANTISLIT=8.000000
_ANALYZER_CODE=0
; None
_DATEMEASURED='08-Jun-2012 20:49:17'
_WL_UNIT='A'
_WL1=1.540600
_WL2=1.544390
_WL3=1.392220
_WLRATIO=0.500000
_ANODE='Cu'
; (Data for Range number 1)
_DRIVE='COUPLED'
_STEPTIME=2124.919922
_STEPSIZE=0.019754
_STEPMODE='C'
_START=5.000000
_THETA=2.500000
_2THETA=5.000000
_KHI=0.000000
_PHI=0.000000
_X=0.000000
_Y=0.000000
_Z=0.000000
_DIVERGENCE=0.000000
_ANTISCATTER=0.000000
_DETECTOR=5
_DETECTORSLIT='unkn'
_AUX1=0.000000
_AUX2=0.000000
_AUX3=0.000000
_TIMESTARTED=9.000000
_TEMPERATURE=26.489990
_TEMP_RATE=0.000000
_TEMP_DELAY=-1.000000
_KV=40
_MA=40
_RANGE_WL=1.540600
_3DPLANE=0
_GONIOMETER=3.250200
_PSDCHANNEL0=0
_2THETACPS
还是他数据本身有问题?请知道的网友帮忙看一下,谢谢