主题:【求助】ICPE9000

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小菜鸟??
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作为一个新手,最近接管了一台ICPE9000,请问微波消解后的消解罐浸泡在多大浓度的硝酸中
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JOE HUI
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ISO8124-5有讲到,10%体积比的硝酸浸泡器皿消解罐等,至少浸泡2个小时
引用原文:5.2 Apparatus
All glassware shall be soaked in 10 % (v/v) nitric acid (5.1.2) for at least 2 h and then rinsed in deionised
water before use.
5.1.1 Nitric acid, concentrated, 1,40 g/ml, 65 % (v/v), “analytical” grade.分析纯级别的硝酸,质量分数65%
5.1.2 Nitric acid, 10 % (v/v): Add 100 ml concentrated nitric acid (5.1.1) to 500 ml water (5.1.4). Dilute
to 1 000 ml with water (5.1.4).10%体积比的硝酸浸泡液
5.1.4 Water, of at least grade 3 purity, in accordance with ISO 3696.水要满足ISO3696(等同GB6682的三级水要求)
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2019/3/4 15:29:12 Last edit by xurunjiao5339
砂锅粥
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想要效果好一点就增大浓度,勤换酸液。
消解罐切记不要用东西刷,平时洗都是用水冲就行,内壁如果变粗糙的话以后就很难洗干净了。
jxkzkksskksks
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原文由 JOE HUI(xurunjiao5339) 发表:ISO8124-5有讲到,10%体积比的硝酸浸泡器皿消解罐等,至少浸泡2个小时引用原文:5.2 ApparatusAll glassware shall be soaked in 10 % (v/v) nitric acid (5.1.2) for at least 2 h and then rinsed in deionisedwater before use.5.1.1 Nitric acid, concentrated, 1,40 g/ml, 65 % (v/v), “analytical” grade.分析纯级别的硝酸,质量分数65%5.1.2 Nitric acid, 10 % (v/v): Add 100 ml concentrated nitric acid (5.1.1) to 500 ml water (5.1.4). Diluteto 1 000 ml with water (5.1.4).10%体积比的硝酸浸泡液5.1.4 Water, of at least grade 3 purity, in accordance with ISO 3696.水要满足ISO3696(等同GB6682的三级水要求)
好的,谢谢
dadgoh
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zyl3367898
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wangjunyu
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购置一个酸缸配置10的酸,使用完的器皿先用自来水清洗干净,再放进去浸泡。
jxkzkksskksks
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原文由 JOE HUI(xurunjiao5339) 发表:ISO8124-5有讲到,10%体积比的硝酸浸泡器皿消解罐等,至少浸泡2个小时引用原文:5.2 ApparatusAll glassware shall be soaked in 10 % (v/v) nitric acid (5.1.2) for at least 2 h and then rinsed in deionisedwater before use.5.1.1 Nitric acid, concentrated, 1,40 g/ml, 65 % (v/v), “analytical” grade.分析纯级别的硝酸,质量分数65%5.1.2 Nitric acid, 10 % (v/v): Add 100 ml concentrated nitric acid (5.1.1) to 500 ml water (5.1.4). Diluteto 1 000 ml with water (5.1.4).10%体积比的硝酸浸泡液5.1.4 Water, of at least grade 3 purity, in accordance with ISO 3696.水要满足ISO3696(等同GB6682的三级水要求)
机器上的炬管等也是采用10%硝酸浸泡吧?
JOE HUI
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原文由 jxkzkksskksks(Insm_d6ae4416) 发表:机器上的炬管等也是采用10%硝酸浸泡吧?
王水,一般新制的王水浸泡炬管
tang566
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10%(体积比)硝酸溶液,浸泡8小时,然后再用清水清洗,用三级水润洗。
手机版: ICPE9000
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