主题：【讨论】稻瘟灵残留分析方法翻译求证

原文由 redanqi 发表:
提取
称取20.0g经粉碎并过20目筛的大米样品置具塞锥形瓶中，加入50mL丙酮，于电动振荡器上振荡30min，用快速定性滤纸过滤于烧杯中，残渣再用30mL丙酮按上法再提取一次。用30mL丙酮分次洗涤残渣，洗液并入烧杯中，于水浴（50℃）上挥发浓缩近干。

3.1 Extraction
Weigh 20g of rice sample grinded and passed the 20 mesh sieve to a flask with stopper, add 50 ml of acetone, shake for 30 minutes by the electrodynamic shaker, filter to a beaker through quick qualitative filter paper, extract the residue once more using the above method by 30 ml of acetone. Wash the residue by 30 ml of acetone in several times, combine the washings to a beaker, vaporize to dry on the water bath of 50℃.

3.1 Extraction
Weigh 20.0g of ground rice sample that passes 20 mesh to a conical flask with stopper. Add 50 ml of acetone and shake for 30 minutes with electric shaker(agitator). The mixture is then filtered to a beaker through quick qualitative filter paper, and the residue will be extracted once more using the above mentioned method through 30 ml of acetone. Wash the residue through (by) 30 ml of acetone in several times, combine the washings to a beaker, vaporize to dryness in the water bath at 50℃.

原文由 ruojun 发表:

原文由 redanqi 发表:
提取
称取20.0g经粉碎并过20目筛的大米样品置具塞锥形瓶中，加入50mL丙酮，于电动振荡器上振荡30min，用快速定性滤纸过滤于烧杯中，残渣再用30mL丙酮按上法再提取一次。用30mL丙酮分次洗涤残渣，洗液并入烧杯中，于水浴（50℃）上挥发浓缩近干。

3.1 Extraction
Weigh 20.0g of ground rice sample that passes 20 mesh to a conical flask with stopper. Add 50 ml of acetone and shake for 30 minutes with electric shaker(agitator). The mixture is then filtered to a beaker through quick qualitative filter paper, and the residue will be extracted once more using the above mentioned method through 30 ml of acetone. Wash the residue through (by) 30 ml of acetone in several times, combine the washings to a beaker, vaporize to dryness in the water bath at 50℃.

原文由 redanqi 发表:
提取
称取20.0g经粉碎并过20目筛的大米样品置具塞锥形瓶中，加入50mL丙酮，于电动振荡器上振荡30min，用快速定性滤纸过滤于烧杯中，残渣再用30mL丙酮按上法再提取一次。用30mL丙酮分次洗涤残渣，洗液并入烧杯中，于水浴（50℃）上挥发浓缩近干。

3.1 Extraction
Weigh 20.0g of ground rice sample that passes 20 mesh to a cornial flask with stopper. Add 50 ml of acetone and shake for 30 minutes with electric shaker(agitator). The mixture is then filtered to a beaker through quick qualitative filter paper, and the residue will be extracted once more using the above mentioned method through 30 ml of acetone. Wash the residue through (by) 30 ml of acetone in several times, combine the washings to a beaker, vaporize to dryness in the water bath at 50℃.
非常感谢.
但是为什么大部分句子用主动式The mixture is then filtered 用被动式??

原文由 redanqi 发表:
层析柱（φ20mm×200mm）下端装入2cm高的无水硫酸钠，称取10 g硅镁吸附剂装入层析柱，柱上端再装2cm高的无水硫酸钠
Pack the column ( Φ20mm x200mm) with 2 cm of anhydrous sodium sulfate, 10 g of silicon-magnesium adsorbent, and 2 cm of anhydrous sodium sulfate in consequence.个人觉得这样翻译简洁些,但不知道专业上有没有这样的说法,这还得请教茅茅姐.
茅茅姐不回答，我说：Pack the column ( Φ20mm x200mm) with 2 cm of anhydrous sodium sulfate at the bottom, followed by 10 g of silicon-magnesium adsorbent, then 2 cm of anhydrous sodium sulfate again in the upper end.

原文由 happyjyl 发表:
用少量二氯甲烷溶解样品提取浓缩液-Dissolve the concentration of the extract with a little amount of dichloromethane

减压浓缩-concentrate under reduced pressure

继续浓缩至1.0mL以下-concentrate to less than 1.0 ml

原文由 ruojun 发表:

原文由 redanqi 发表:
层析柱（φ20mm×200mm）下端装入2cm高的无水硫酸钠，称取10 g硅镁吸附剂装入层析柱，柱上端再装2cm高的无水硫酸钠
Pack the column ( Φ20mm x200mm) with 2 cm of anhydrous sodium sulfate, 10 g of silicon-magnesium adsorbent, and 2 cm of anhydrous sodium sulfate in consequence.个人觉得这样翻译简洁些,但不知道专业上有没有这样的说法,这还得请教茅茅姐.
茅茅姐不回答，我说：Pack the column ( Φ20mm x200mm) with 2 cm of anhydrous sodium sulfate at the bottom, followed by 10 g of silicon-magnesium adsorbent, then 2 cm of anhydrous sodium sulfate again in the upper end.

原文由 ruojun 发表:

原文由 happyjyl 发表:
用少量二氯甲烷溶解样品提取浓缩液-Dissolve the concentration of the extract with a little amount of dichloromethane

减压浓缩-concentrate under reduced pressure

继续浓缩至1.0mL以下-concentrate to less than 1.0 ml

减压浓缩-concentrate under reduced pressure是真空浓缩么：vacum concentrated??