主题:【求助】求有脉冲安培检测器的代检单位

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lvxiumei
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因化学原料药出口,需要依照国外药典检测组分和杂质,相关仪器要求如下,希望有能力的检测单位留下联系方式,或者和我联系0755-26514276,QQ34498139,谢谢大家!

Column:
— size: l =0.25m, Ф=4.6mm,
— stationary phase: styrene-divinylbenzene copolymer R (8 μm) with a pore size of 100 nm,
— temperature: 55°C

Post-column solution: a carbonate-free sodium hydroxide solution diluted 1 to 25, previously degassed, which is added pulse-less to the column effluent using a 375 μl polymeric mixing coil.

Detection: pulsed amperometric detector or equivalent with a gold indicator electrode, a silver-silver chloride reference electrode, and a stainless steel auxiliary electrode which is the cell body, held at respectively + 0.05 V detection, + 0.75 V oxidation and 0.15 V reduction potentials, with pulse durations according to the instrument used.
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yfytap
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恐龙
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是批量做吗,做课题研究否,可考虑。普通测试不做。
qiuhaitang
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做抗生素,应该是批量做的,如果一直需要出口的话,呵呵,不过样品测试费用很贵的。因为这个方法用的液相色谱柱坏得快,最好能由测样单位提供色谱柱。
因为方法比较老,用的糖三电位波形,对电极的伤害也相对要大一些,另外方法所用的金电极是3mm的。
原文由 恐龙(konglong) 发表:
是批量做吗,做课题研究否,可考虑。普通测试不做。
qiuhaitang
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这个方法做起来并不是很容易,而且跟所需检测的类型有关,建议找一个做安培检测经验丰富的实验室来做。

原文由 lvxiumei(lvxiumei) 发表:
因化学原料药出口,需要依照国外药典检测组分和杂质,相关仪器要求如下,希望有能力的检测单位留下联系方式,或者和我联系0755-26514276,QQ34498139,谢谢大家!

Column:
— size: l =0.25m, Ф=4.6mm,
— stationary phase: styrene-divinylbenzene copolymer R (8 μm) with a pore size of 100 nm,
— temperature: 55°C

Post-column solution: a carbonate-free sodium hydroxide solution diluted 1 to 25, previously degassed, which is added pulse-less to the column effluent using a 375 μl polymeric mixing coil.

Detection: pulsed amperometric detector or equivalent with a gold indicator electrode, a silver-silver chloride reference electrode, and a stainless steel auxiliary electrode which is the cell body, held at respectively + 0.05 V detection, + 0.75 V oxidation and 0.15 V reduction potentials, with pulse durations according to the instrument used.
恐龙
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做是可以做, 但柱后衍生的安培检测成本很高,柱子和电极消耗快。这个欧洲标准就是烦。
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