主题:【我的“小屋”秀】xmciq-食品理化实验室-鼓浪屿旁边的家

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本人帖子只是介绍实际情况,以实名方式介绍国家对进出口食品安全的支持和厦门局食品实验室取得的工作成绩,如果因为各种非技术内容的负面评论给我带来工作关系上的负担和领导的“关心”,我只能毫不犹豫的删帖,请各位论坛朋友发表评论时手下留情,

言论自由,但是在这里,只是讨论技术,交流技术的地方,我自身的发言也只是出于技术,介绍国内技术方面的最新进展、信息和先进经验,有没有回复我都不看重的,作为小小的技术人员做好自己的技术工作就是自己最大的本分,网友的回复既是支持也可能是对我的暗箭伤害。

所以在这里不要讨论社会民生问题,这里只是讨论技术问题,避免最坏情况导致我删帖的结果。谢谢支持,请回帖前三思!


嵩屿,位于厦门海沧,与鼓浪屿隔海(~1KM)相望,是我们实验室所在。
厦门局(xmciq)作为正厅单位,下属技术中心属于正处级事业单位,本人所在为食品理化实验室,位于化学楼的4楼和5楼,这里是我工作和“战斗”的地方,在这里度过了无数个辛苦的夜晚,常常来袭的食品安全突发事件是我们工作中最大的挑战,这里有我共同奋斗的同事,这里是我事业扎根的地方,这里是我的家,欢迎您来参观,欢迎就科研,课题展开技术合作。下面我荣幸为您一一介绍。
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Song , located in Xiamen Haicang, and Gulangyu across (~ 1KM) , is where our laboratory.
Xiamen Entry-Exit Inspection and Quarantine Bureau of the People's Republic of China,Inspection and
Quarantine Technology Center. where my physical and chemical laboratory for the food, chemical building
at 4th floor and 5th floor, where I work and the "battle"  place where through so many hard nights,
often attacking the food safety emergency is the greatest challenge in our work, here are my colleagues
in the common struggle, here is the root cause of where I am, here is my home, welcome to visit,
welcomed the research, issues in technical cooperation. Here I am honored to introduce to you one by one.

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2009年5月8日温家宝总理视察厦金航线检验检疫工作
May 8, 2009 Premier Wen Jiabao visited the Xiamen-Kinmen route inspection and quarantine work



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2010年2月14日,胡锦涛主席到厦金航线口岸视察厦门检验检疫工作
February 14, 2010, President Hu Jintao to visit Xiamen, Xiamen-Kinmen route port inspection and quarantine

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1 技术中心简介 http://www.xmciqtech.gov.cn/Article_Index.asp
厦门出入境检验检疫局检验检疫技术中心(以下简称技术中心)是经国家批准设立的独立注册的事业法人单位,隶属于厦门出入境检验检疫局。主要从事机电产品、食品、农产品、动植物及其产品、化矿金产品、包装材料等的检验检测业务,以及科研制标、检测技术开发、技术咨询、培训等工作。
技术中心下设7个实验室、1个分中心和3个管理部门。分别为电气实验室(国家级电气安全检测实验室)、植物检疫实验室(国家级蔬菜种子与植物种传病毒检疫实验室)、食品理化实验室、微生物实验室、动物检验检疫实验室、化矿金化学实验室、金属及包装实验室;同安分中心;以及业务开发部、综合管理部、财务部(详见图1组织机构图)。
经过几十年建设,技术中心已具备了雄厚的检测实力。拥有先进的检测设备和大型分析仪器1000余台套,价值1亿余元,其中包括API5000液质联用仪液相飞行时间质谱仪、三重四极杆气质联用仪、基质辅助激光解析电离-飞行时间质谱、电感耦合等离子体质谱仪、激光共聚焦扫描显微镜、X射线荧光光谱仪、X射线衍射仪、四极杆单级气质联用仪、DNA测序仪、全自动微生物鉴定仪、变性高效液相色谱仪、电感耦合等离子体发射光谱仪、直读光谱仪、傅里叶红外光谱仪、台式电子扫描显微镜、EMI电磁兼容接收机、EMS辐射抗扰度测试仪、二次电池充放电测试仪、高纯锗γ能谱仪、液相色谱仪气相色谱仪原子吸收分光光度计、原子荧光形态分析仪、离子色谱仪、热释光检测仪等国际最先进的仪器设备及3米法电波暗室、植物病毒检疫隔离温室等先进的检测设施。除了一流的仪器设备外,技术中心还汇集了一支具有高学历、经验丰富的骨干科技人员队伍,其中博士11名、在读博士2名、硕士23名,高级职称人员32人(包括研究员3人),中级职称38人。实验室面积达1万2千多平方米,其中面积一万平方米的海沧新实验大楼已于2008年8月25日启用。新建的实验大楼,实验环境得到极大改善,实验设施得到全面更新,新购的十几台大型已安装调试完毕并投入使用,实验室检测水平进一步提升。
目前的技术中心已成为厦门市乃至闽南地区最大的机电产品、食品、动植物及其产品、化矿金产品和包装材料的专业检测机构。掌握着最新的检测方法,拥有ISO、GB、JIS、ASTM、IEC、EN、SN等国内外最新的检测方法。技术中心以“科学严谨、公正准确、优质高效、竭诚服务”为宗旨,按照ISO/IEC 17025标准建立、实施并保持符合实验室工作范围的质量管理体系,站在第三方公正立场,独立开展各项检验/检测工作,出具检验报告。
2 技术中心实验室先后取得以下资质和认可
— 中国合格评定国家认可委员会( CNAS)认可
— 国家计量认证合格 (CMA)检验单位
— 国家科委认定的科技成果检测鉴定国家级检测机构
— 国家认监委批准的转基因产品检测实验室
— 福建省治理 “ 餐桌污染 ” 食品安全指标监测评价质检机构
— 日本厚生省注册登记认可和韩国食药厅认可的食品检验实验室
— 国家质检总局指定的进出口化妆品专项检测实验室
— 国家质检总局指定的电池汞含量检测实验室 
— 国家质检总局指定的进口涂料有害物质专项检测实验室
— 国家质检总局指定的木制品甲醛专项检测实验室
— 金伯利进程毛坯钻石指定检验机构
— 电子产品 3C认证实验室
— 中国质量认证中心( CQC)授权的产品自愿认证指定实验室
— 福建省人民法院鉴定人
该帖子作者被版主 titi10积分, 2经验,加分理由:实验室从无到有就像一个新生命诞生一样可贵
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厦门农产品技术中心与安捷伦合作开展鱼种贝类鉴定研究
Agricultural Technology Center in Xiamen in collaboration with Agilent identification of species of shellfish
http://www.instrument.com.cn/news/20100510/042141.shtml

质检总局09年批准筹建66家国家检测重点实验室
General Administration in 2009 approved the establishment of 66 State Key Laboratory testing
http://www.instrument.com.cn/news/20100318/040113.shtml

2010年01月07日厦门出入境检验检疫系统2009年科学发展工作述评
January 7, 2010 Xiamen Entry-Exit Inspection and Quarantine system work 2009 Review of Scientific Development
http://finance.sina.com.cn/roll/20100107/08543173593.shtml

3 食品检测部分
    (1)主要的业务内容:食品、动植物及其产品的微生物检验,农药残留量、兽药残留量、重金属、毒素等有毒有害物质检验和食品添加剂检验,食品的毒理学检验,转基因产品的检测以及动植物传染病、寄生虫病、病虫、杂草等有害生物的检疫,食品容器及食品包装材料安全卫生检验。
(2)承检实验室:技术中心承担食品、食品容器、食品包装材料、动植物及其产品检测的实验室:食品理化实验室、微生物实验室、植物检疫实验室、动物检验检疫实验室、化矿金化学实验室。
(3)实验室检测业绩:2006~2009年承检上述工作的情况大致如下:
①涉及的种类:饼干糕点,糖及糖果,酒,饮料,调味品,罐头食品,蔬菜,真菌蘑茹类,粮食、植物淀粉及制品,水产品,动物肉及制品,食品添加剂,乳与乳制品,动植物油脂,蛋及蛋制品,以及食品用容器(陶瓷类,塑料类,金属类、纸制品类和竹木制品类等)和食品包装材料等,共约300多个品种。
②主要检验的项目:食品化学项目(重金属,农药残留,兽药残留,毒素等有害物质,食品添加剂以及其它一些常规化学分析项目)约123553项次;微生物检验项目(细菌总数、大肠杆菌、各种致病菌和转基因产品检测)约25668项次;动植物检疫检验项次约26858项次。
(4)主要的分析和检测设备:液相串联质谱仪(LC-MS-MS, 3台), 液相飞行时间质谱仪(1台),气相色谱仪(GC,多台)、气质联用仪(GC-MS,多台)、高效液相色谱仪(HPLC,多台,美国安捷伦公司,美国PE公司)、原子吸收分光光度计(AAS,2台)、原子荧光分光光度计(AFS)、荧光PCR仪(Sequence Detection System (Fluorescence Quantitative PRC  System),美国Applied Biosystems公司)、凝胶图像分析系统(Gel Documentation and Analysis System 厂商:英国Uvilec.co.uk)自动微生物检测系统(VITEK AUTOMICROBIC SYSTEM ,厂商:BIO MERIEUX VITEK INC.U.S.A)、酶标仪(Microplate reader  厂商:美国Bio-Rad公司)等各类先进的分析检测仪器60多台。
(5)实验室设施情况:检验用房面积约2000多平方米,设置有专用的微生物、食品化学、转基因、毒理等方面的检验检疫设施。
(6)实验室近年来参加的能力验证情况:近年来共参加食品和动植物产品中农兽残、重金属、微生物、病原菌、转基因等相关领域40次能力验证,结果均为满意,见表1;参加实验室间比对4次,结果均为满意,见表2。
4 技术中心动物源性残留监控
(1)组织结构
技术中心是国家质检总局指定的35个残留监测实验室之一,承担着厦门局辖区内的残留监控样品的检测任务。

技术中心平面效果图Technology Center Graphic renderings



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鸟瞰Bird's eye view


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中心动工前,打地基,右上角,吊塔下的岛为鼓浪屿
Center prior to the commencement upper right corner hit the foundation, under the hanging tower island Gulangyu

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2008年夏天,中心完工。远方背景为厦门岛东渡区域,右上角的岛为鼓浪屿
The summer of 2008, the Center completed. Going the distance the background for the area of Xiamen Island, the upper right corner of the island as Gulangyu

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2008.9.8,厦门九八贸洽会前落成

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中心楼群封顶仪式for blocks of cap ceremony

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办公室,墙刚刚砌好的时候。Office, when the wall just finish


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装修好的办公室A furnished office

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2010/5/13 10:43:58 Last edit by enhua
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1 Technical Introduction http://www.xmciqtech.gov.cn/Article_Index.asp
Xiamen Inspection & Quarantine Technology Center (hereinafter referred to Technology Center) is a state approved the establishment of an independent cause of registered legal entities, Xiamen Entry-Exit Inspection and Quarantine under. Mainly engaged in mechanical and electrical products, food, agricultural products, plants and animals and their products, products of gold mining, packaging materials, inspection and testing services, etc., as well as research and manufacturing standard, test technology development, technical consulting, training and so on.
Technology Center consists of seven laboratories, a sub-centers and three administrative departments. Electrical Laboratory, respectively (National Electrical Safety testing laboratory), Plant Quarantine Laboratory (National Vegetable Seed and Plant Quarantine Laboratory seed-borne virus), food physics and chemistry laboratory, microbiology laboratory, animal inspection and quarantine laboratory, gold mine of chemical laboratory, metals and packaging laboratories; with the law-abiding center; and business development, general management, finance (see Figure 1 Organization Chart).

现在开始介绍实验室了
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2004年巴西“种衣剂”大豆事件中 ,登轮检查种衣剂大豆,7舱,5万吨,在旧实验楼。
2004 Brazil "Seed" soybean event, board the vessel inspection of soybean seed coating

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旧技术中心实验楼Old Laboratory Building Technology Center

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旧楼实验室照片回忆Memories of old lab photos

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旧楼实验室残留分析试验台Residue analysis laboratory test table of old buildings

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下面开始介绍新楼实验室The following laboratory began on the new floor


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搬家前的走廊Corridor before moving

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气瓶室Cylinder chamber


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气体通过管路送到仪器Gas delivered by pipeline equipment


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样品制备,研磨。细磨;Sample preparation, grinding. Fine grinding;


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粗磨Coarse grinding



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前处理间Pre-treatments



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通风橱aerator 


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2010/5/13 10:26:11 Last edit by enhua
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After several years of construction, technology center already has a solid detection capabilities. Advanced testing equipment and a large analysis of more than 1,000 sets of equipment, worth 100 million yuan, including API5000 LC-MS-MS, liquid time of flight mass spectrometer, triple quadrupole GC-MS, matrix-assisted laser desorption ionization - time of flight mass spectrometry, inductively coupled plasma mass spectrometry, confocal laser scanning microscopy, X-ray fluorescence spectrometer, X-ray diffraction, single-stage quadrupole GC-MS, DNA sequencer, automated microbial identification instrument, Denaturing high liquid chromatography, inductively coupled plasma emission spectrometry, direct-reading spectrometer, Fourier transform infrared spectroscopy, desktop scanning electron microscope, EMI Receivers EMC, EMS radiation immunity tester, rechargeable battery discharge tester HPGe γ spectrometry, liquid chromatography, gas chromatography, atomic absorption spectrometry, atomic fluorescence morphological analyzer, ion chromatograph, thermoluminescence detectors and other international most advanced equipment and 3m wave darkroom, greenhouse plant quarantine viruses and other advanced testing facilities. In addition to first class equipment, the technology center also brings together a highly educated and experienced team of key technical personnel, including 11 PhD in PhD 2, MA 23, senior professional titles, 32 people (including fellow 3 ), intermediate grade 38. Laboratory area of 10 002 more than 1000 square meters, of which an area of 10,000 square meters of new laboratory building was Haicang August 25, 2008 opening. The new laboratory building, experimental environment has been greatly improved laboratory facilities are fully updated, new large-scale purchase of a dozen units have been installed and adjusted and put into use, to further enhance the level of laboratory testing.
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旋转蒸发仪,现在残留分析比较少用,毒理实验项目同事比较常用。Rotary Evaporator,


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固相萃取,手动灵活,好用Solid phase extraction, manual and flexible, easy to use


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恒温振荡Temperature oscillation


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平行蒸发,大体积提取浓缩,好用。Parallel evaporation, mass extraction and concentration, easy to use



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氮吹仪:30ml*5通道*10个口,最常用,液氮供气,便宜。缺点:体积限制。
Nitrogen blowing instrument: 30ml * 5 channels * 10 I, the most commonly used liquid nitrogen gas, cheap. Disadvantages: size limit.


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超临界Supercritical

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超临界SFE,SFE Supercritical


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快速溶剂萃取ASE,Accelerated solvent extraction ASE

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GPC,凝胶渗透


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搬到新楼后增加GPC浓缩装置。

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吉尔森固相萃取Gilson SPE

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2010/5/13 10:29:53 Last edit by enhua
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Current technology centers as well as Fujian, Xiamen City has become the largest mechanical and electrical products, food, animals and plants and their products, chemical products and packaging materials, gold mining professional testing organization. Holds the latest detection methods, with ISO, GB, JIS, ASTM, IEC, EN, SN, etc. are the latest detection methods. Technology Center of "scientific rigor, fair and accurate, high quality and efficient and dedicated service", in accordance with ISO / IEC 17025 standard to establish, implement and maintain consistent with the scope of laboratory quality management system, standing on third-party impartiality, independence to carry out the entry inspection / testing work, a survey report.
2 Technical Center laboratory has obtained the following qualifications and accreditation - China National Accreditation Board for Conformity Assessment (CNAS), - National Measurement Certification Compliance (CMA) test unit - the State Science Commission finds that the scientific outcome identification of national testing organizations - national identity monitoring Committee approval of GMO testing laboratory - Fujian Province governance "table pollution," Evaluation of quality control indicators for monitoring food safety agency - Japan Ministry of Health registration Korean Food and Drug Administration approved and accredited food testing laboratory - into the designated AQSIQ special export cosmetic testing laboratories - AQSIQ designated testing laboratory mercury content
Food testing part 3
(1) Major Business: food, animals and plants and their products of microbial testing, pesticide residues, veterinary drug residues, heavy metals, toxins and other toxic substances testing and inspection of food additives, food toxicology testing, genetically modified products Detection of animal and plant diseases, parasitic diseases, pests, weeds and other pests of quarantine, food containers and food packaging materials safety and health inspection.
(2) principal inspection laboratory: Technical Center has food, food containers, food packaging materials, animals, plants and product testing laboratories: Food physics and chemistry laboratory, microbiology laboratory, plant quarantine laboratory, animal inspection and quarantine laboratories chemical laboratory of mining gold.
(3) laboratory test results: review 2006 to 2009 bearing the above-mentioned is as follows:
① species involved: biscuit cake, sugar and sweets, alcohol, beverages, condiments, canned food, vegetables, fungi, mushroom type, food, starch and plant products, aquatic products, animal meat and products, food additives, milk and milk products, animal fat, eggs and egg products, and food with a container (ceramic, plastic, metal, paper and wood products category, etc.) and food packaging materials, a total of about 300 species.
- AQSIQ import of specified hazardous substances in the special paint testing laboratories - AQSIQ formaldehyde wood products designated by special testing laboratory - the Kimberley Process rough diamond designated inspection agencies - Electronics Lab 3C Certification - China Quality Certification Centre (CQC) voluntary certification of products authorized by the designated laboratories - Fujian Province People's Court expert

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常规设备General Equipment
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pH计,pH meter


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自动滴定Automatic titration


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高温室Oven

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烘箱

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马弗炉Muffle furnace.

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FOSS,定氮仪FOSS, Nitrogen Determination Apparatus


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FOSS,脂肪测定仪FOSS, fat analyzer

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分光光度计Spectrophotometer

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2010/5/13 10:34:08 Last edit by enhua
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② major test of the project: Food Chemistry project (heavy metals, pesticides, animal drug residues, toxins and other harmful substances, food additives, and other routine chemical analysis of the project) about 123 553 Ci; microbiological test items (the total number of bacteria, E. coli, the pathogens and GMO detection) is about 25,668 times; animal and plant quarantine inspection of about 26,858 times entry times.
(4) the main analysis and testing equipment: liquid tandem mass spectrometry (LC-MS-MS, 3 units), time of flight mass spectrometry Liquid (1 unit), gas chromatography (gc, more than one), gc meter (gc-MS, multiple), high performance liquid chromatography (HPLC, more than the United States Agilent, U.S. PE firm), atomic absorption spectrophotometer (AAS, 2 sets), atomic fluorescence spectrometry (AFS) fluorescence PCR instrument (Sequence Detection System (Fluorescence Quantitative PRC System), the United States Applied Biosystems Inc.), gel image analysis system (Gel Documentation and Analysis System Manufacturers: British Uvilec.co.uk) automatic microbial detection system (VITEK AUTOMICROBIC SYSTEM, Manufacturers: BIO MERIEUX VITEK INC.USA), microplate reader (Microplate reader manufacturers: the United States Bio-Rad Corporation) and other kinds of advanced testing instruments more than 60.
(5) laboratory facilities: The test covers a floor space of 2,000 square meters, set up a dedicated micro-organisms, food chemistry, transgenic, toxicological aspects of inspection and quarantine facilities.
(6) participate in proficiency testing laboratory in recent years: The years of middle peasants to participate in animal food and animal and plant products residues, heavy metals, microbes, pathogens, genetically modified and other related fields 40 proficiency testing, the results are satisfactory, see Table 1; participate in inter-laboratory comparison 4 times and the results are satisfactory, in Table 2.
4 technical centers residue monitoring of animal origin (1) Structure Technology Center is designated by the State Administration of Quality Supervision 35 one residue monitoring laboratory, undertaking Xiamen Council area of residue monitoring samples detection tasks.

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古老的岛津,填充柱气相色谱Shimadzu ,years old, packed column gas chromatography



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古老的5890,手动调节The old 5890, manual adjustment


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gc7890,电子流量控制。 有双塔、双FPD方式。gc7890, electronic flow control


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gc顶空装置Headspace gc devices

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氢气发生器Hydrogen Generator


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单四极杆气质,实验室最早的气质。6、7年前的设备条件很差。
Single quadrupole temperament, the earliest laboratory 6,7 years ago, the equipment condition in poor 


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Varian 320gcMSMS,效果不错,洗源麻烦。Varian 320gcMSMS, good results, wash the source trouble.

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离子肼气质


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agilent1200,2台,配置不同,常压配置。agilent1200, 2 sets of different configurations


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agilent1200正面照

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waters2695,不错。


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离子色谱,测水质项目Ion chromatography, water quality testing project


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2010/5/13 10:39:33 Last edit by enhua
enhua
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5楼 液相液质气相气质,一字排开5th Floor, liquid, liquid mass, gas, temperament, lined up


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API3000


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waters  UPLC-TQD


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waters UPLC-TOF



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API5000用的氮气发生器API5000 with the nitrogen generator


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API5000的机械泵API5000 mechanical pump


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微波消解Microwave digestion


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原子荧光Atomic Fluorescence



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DOS年代的Varian


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崭新的Varian



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agilent 的ICP-MS


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2010/5/13 10:46:46 Last edit by enhua
jmcdcjyk
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〓疯子哥〓
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楼主的仪器很多啊,能简单介绍下实验室的情况么?能简单介绍下仪器的情况么?仪器的型号、检测什么物质?期待楼主持续更新
fyzhong7070
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厦门真有钱,请问楼主实验室装修是哪家公司的,我也在着手理化室的装修
pany
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