主题:【求助】二硫代氨基甲酸酯类农药检测

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lvada
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二硫代氨基甲酸酯类农药 与 氯化亚锡反应时,加热温度应该控制在什么温度?能用其他的还原剂吗?
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原文由 我在故我思(hotdoglet) 发表:
2.2 For Mancozeb in Water
An 8 mL portion of sample was placed into a 40 mL vial along with 10% EDTA, and 3% nCl2/8N HCl solution and capped. The samples were placed in a heating block at 100℃for four hours with shaking at various time intervals. The samples were then analyzed by GC/MSD
using SIM.

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详情请参下贴6、7楼
http://bbs.instrument.com.cn/shtml/20090103/1681211/
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