PDF#87-0712: QM=Calculated; d=Calculated; I=Calculated
Nickel, syn
Ni
Radiation=CuKa1 Lambda=1.54060 Filter=
Calibration= d-Cutoff=17.7 I/Ic(RIR)=7.44
Ref= Calculated from ICSD using POWD-12++ (1997)
Cubic - (Unknown), Fm-3m (225) Z=4 mp=
Cell=3.5238 Pearson=cF4 (Cu)
Density(c)=8.910 Density(m)=8.94A Mwt=58.70 Vol=43.76 F(3)=999.9(.0000,3)
Ref= Swanson, H.E., Tatge, E.
Natl. Bur. Stand. (U.S.), Circ. 539, 359 I1 (1953)
Strong Line: 2.03/X 1.76/4 1.25/2 0.00/1 0.00/1 0.00/1 0.00/1 0.00/1 0.00/1 0.00/1
FIZ=064989: M PDF 00-004-0850.
Calc.
density unusual but tolerable.
No R value given.
At least one TF missing.
See PDF 00-004-0850, 03-065-2865.
Standard X-ray diffraction powder patterns ICSD 43397 and ICSD 44767.
Cell from Acta Crystallogr., 7 464 (1954): 3.5238(3) at 298 K.
a (FM3-M) N
d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d
2.0345 100.0 100.0 1 1 1 3 44.496 22.248 0.2458 3.0884
1.7619 42.0 48.5 2 0 0 4 51.849 25.925 0.2838 3.5661
1.2458 16.1 26.3 2 2 0 8 76.381 38.190 0.4013 5.0433
顺便问一句,你用的是不是PCPDFWIN?因为你说你的只有d值,没有2Theta值。实际上,你按一下字母键d,显示的就是d值,按一下数字键2,显示的就是2Theta值。你试试,免得你下次问相同的问题。