主题:新手求教

浏览0 回复3 电梯直达
cafu2000
结帖率:
100%
关注:0 |粉丝:0
新手级: 新兵
进入ICP-MS样品中含10%或更高的硝酸,对结果会有什么影响?对仪器会有什么负面影响?
另外,手册上说样品中总盐的含量要小于0.2%,如果样品中含有20%左右的硝酸氨或其他氨盐(如氯化铵等),还可以得到好的结果吗?

多谢!
为您推荐
您可能想找: 气相色谱仪(GC) 询底价
专属顾问快速对接
立即提交
renzhihai
结帖率:
100%
关注:0 |粉丝:0
新手级: 新兵
toudada
结帖率:
100%
关注:0 |粉丝:0
新手级: 新兵
原文由 cafu2000 发表:
进入ICP-MS样品中含10%或更高的硝酸,对结果会有什么影响?对仪器会有什么负面影响?
另外,手册上说样品中总盐的含量要小于0.2%,如果样品中含有20%左右的硝酸氨或其他氨盐(如氯化铵等),还可以得到好的结果吗?

多谢!


应该会很损锥吧
如果银子多,可以长期试的
cafu2000
结帖率:
100%
关注:0 |粉丝:0
新手级: 新兵
找到了一个解答:

Total dissolved solids (TDS)

The total amount of material (including major species) in solution in your samples. In general this should be between 0.2% and 0.5%. The general rule for maximum dissolved solids is to consider the boiling point of the matrix oxide; if the matrix oxide is refractory the material is more liable to build up on the cones and the maximum TDS should be kept to 0.2%. If the matrix oxide does not form a refractory oxide, then material is less likely to build up on the cones, and the maximum TDS can be 0.5%. If the matrix forms a gaseous oxide such as with high levels of organic material (ammonium acetate, digested biological material etc.), then the level can go as high as 10%.  As long as the TDS remains within sensible limits the lenses require cleaning routinely for normal sample loads every 6 - 12 months which is the normal preventative maintainance secheduling, outside of this the user should not need to attend to the lens components of the X Series ICP mass spectrometer.

手机版: 新手求教
猜你喜欢最新推荐热门推荐更多推荐
品牌合作伙伴