【HPLC条件】
カラム:CAPCELL PAK C18 MGII
検 出:PDA 230 nm
注入量:5 μL
試 料:【残留農薬試験用試薬】
農薬60成分混合標準溶液I 10 ppm (in Acetonitrile)
農薬12成分混合標準溶液II 10 ppm (in Acetone)
農薬31成分混合標準溶液III 10 ppm (in Acetonitrile)
I, II, IIIを等量混合し,H2Oで2倍に希釈した.
農薬名 分子量 農薬名 分子量 農薬名 分子量
Acephate 183.2 Propamocarb 188.3 Spinosyn A 732.0
Actamiprid 222.7 Pymetrozin 217.2 Spinosyn D 746.0
Acibenzolar acid 180.2 Pyrazolate 439.3 2,3,5-Trimethacarb 193.2
Acibenzolar-S-methyl 210.3 Sethoxydim 327.5 3,4,5-Trimethacarb 193.2
Benzofenap 431.3 Tebufenozide 352.5 Aldicarb 190.3
Carbendazim 191.2 Teflubenzuron 381.1 Aminocarb 208.3
Chlorfluazuron 540.7 Tepraloxydim 341.8 Bendiocarb 223.2
Clethodim 359.9 Tepraloxydim (DMP) 244.3 benfuracarb 410.5
Cumyruron 302.8 Tepraloxydim (OH-DMP) 260.3 Butocarboxim 190.3
Cycloprothrin 482.4 Thiabendazole 201.2 Butocarboxim sulfoxide 206.3
Diflubenzuron 310.7 Thiabendazole metabolite 217.3 Carbaryl 201.2
Dimethirimol 209.3 Tribenuron methyl 395.4 Carbofuran 221.3
Diuron 233.1 Tricyclazole 189.2 Carbofuran-3-hydroxy 237.3
Dymron 268.4 Triflumizole 345.8 Carbosulfan 380.5
Ethoxyquin 217.3 Triflumizole metabolite 294.7 Dioxacarb 223.2
Fenpyroximate(Etype) 421.5 Triforin 435.0 Ethiofencarb 225.3
Fenpyroximate(Ztype) 421.5 Vamidothion 287.3 Fenobucarb 207.3
Fluazinam 465.1 Carpropamid 334.7 Furathiocarb 382.5
Flufenoxuron 488.8 Nitenpyram 270.7 Isoprocarb 193.2
Hexythiazox 352.9 Benzobicyclon 447.0 Mercaptodimetur 225.3
Imazalil 297.2 Benzobicyclon metabolite 354.8 Methomyl 192.2
Imibenconazole 411.7 Cyazofamid 324.8 Metolcarb 165.2
Imidacloprid 255.7 Fentrazamid 349.8 Oxamyl 219.3
Inabenfide 338.8 Methoxyfenozide 368.5 Pirimicarb 238.3
Isouron 211.3 Tepraloxydim metabolite 357.8 Promecarb 207.3
Linuron 249.1 1-Naphthylacetic acid 186.2 Propoxur 209.2
Mepanipyrim 223.3 Acequinocyl 384.5 Terbucurb 277.4
Mepanipyrim metabolite 243.3 Acequinocyl hydroxy 342.5 Thiodicarb 354.5
Methabenzthiazuron 221.3 Azocyclotin 436.2 Thiofanox 218.3
Methamidophos 141.1 Cartap hydrochloride 273.8 Thiofanox sulfone 250.3
Oxaziclomefone 376.3 Cyhexatin 385.2 Thiofanox sulfoxide 234.3
Pencycuron 328.8 Daminozid 160.2 MPMC 179.2
Phoxim 298.3 Fenbutatin oxide 1052.7 XMC 179.2
Probenazole 223.2 Lufenuron 511.2 ※表示分子量は平均分子量
Prochloraz 376.7 Thiocyclam 271.4