各位大哥大姐大叔大妈，小弟有一篇关于伏虫隆分析方法的英文资料，跪求翻译，不胜感激！
1..Determination of Diflubenzuron and Teflubenzuron in Fish Feed By High Performance Liquid Chromatography
Authors: Victor Hormazabal; Magne Yndestad
Abstract
A simple method for the determination of diflubenzuron and teflubenzuron in fish feed by HPLC is presented. The samples were extracted with acetone - tetrahydrofurane and diluted with tetrahydrofurane, prior to the HPLC. The lower limit of quantification was 0.25 and 0.4 g/kg. for diflubenzuron and teflubenzuron in fish feed, respectively.

2.Determination of seven benzoylphenylurea insecticides in processed fruit and vegetables using high-performance liquid chromatography/tandem mass spectrometry
Anna Sannino, Mirella Bandini

Abstract
A liquid chromatographic method with electrospray ionization tandem mass spectrometry (LC/ESI-MS/MS) has been developed for the sensitive and selective determination of seven benzoylphenylurea insecticide residues (diflubenzuron, triflumuron, lufenuron, flufenoxuron, teflubenzuron, chlorfuazuron, hexaflumuron) in pear baby purée, concentrated lemon juice, and tomato pulp. The general sample extraction/partition method for our established multiresidue methods has been used. The entire procedure involves extraction of residues with acetone and partition into ethyl acetate/cyclohexane. Chromatographic determination was performed using a C18 column and isocratic elution. Fourteen MS/MS transitions of precursor ions were monitored (two for each pesticide) using negative ESI. The majority of mean recoveries at fortification levels of 0.002-0.020 and 0.020-0.200 mg/kg were in the range 77-102% with relative standard deviations between 2 and 10%. The excellent sensitivity and selectivity of this LC/MS/MS method allowed quantitation and identification at low levels in difficult matrices with a run time of 4 min.

3.High-performance liquid chromatographic determination of benzoylurea insecticides residues in grapes and wine using liquid and solid-phase extraction
George E. Miliadisa, Nicholas G. Tsiropoulosb, , and Pipina G. Aplada-Sarlisa
Abstract
A method for the determination of the benzoylurea insecticides diflubenzuron, triflumuron, teflubenzuron, lufenuron and flufenoxuron in grapes and wine by HPLC has been developed and validated. Grape samples (50 g) were homogenized and extracted with ethyl acetate–sodium sulfate and further cleaned-up by solid-phase extraction on silica sorbent. Wine samples (10 ml) diluted with water (1:3) were solid-phase extracted on an octadecyl sorbent using methanol as the eluent. The pesticides were separated on a reversed-phase octadecyl narrow-bore column by gradient elution and the residues were determined with a UV diode array detector. The calibration plots were linear over the range 0.05–5 μg/ml. Recoveries of benzoylurea pesticides from spiked grapes (0.02–2.0 mg/kg) and wine (0.01–0.2mg/l) were 85.8–101.6% and 69.1–104.8%, respectively, and the limits of quantification for these insecticides were <0.01 mg/kg for grapes and <0.01 mg/l for wine. The method was applied to the determination of flufenoxuron and teflubenzuron residues in grapes from treated fields and in produced wine.

4. SFC-UV determination of diflubenzuron residues, teflubenzuron and triflumuron in apple and pear pulps for baby food
C. Bicchi, C. Balbo, A. D'Amato and O. Panero
Summary A method to determine residues of diflubenzuron (DFB), teflubenzuron (TFB), triflumuron (TFM) at 0.01 ppm with recoveries above 60% in apple and pear pulps for baby food is described. DFB, TFB and TFM are extracted with methanol, and cleaned up by SPE using C18 stationary phase and methanol mobile phase. Analysis of the three pesticides is by SFC-UV at 254 nm using a Diol column, and CO2 at 30 MPa and 40°C modified with acetonitrile (10%) mobile phase.

推荐答案：xyclczy回复于2008/05/05

1 ..测定灭幼脲和伏虫隆在鱼饲料的高效液相色谱分析
作者：维克托hormazabal ; magne德斯达德
摘要
一个简单的方法，用于测定灭幼脲和伏虫隆在鱼饲料的高效液相色谱分析介绍。样本提取，用丙酮-t etrahydrofurane和稀释t etrahydrofurane，事先向高效液相色谱法。定量下限为0.25和0.4 g / kg组。为除虫脲和伏虫隆在鱼饲料，分别。

2.determination 7 benzoylphenylurea杀虫剂在加工水果和蔬菜使用高高效液相色谱/串联质谱
安娜圣尼诺， mirella bandini

摘要
一高效液相色谱法与电喷雾串联质谱（立法会/电喷雾质谱/女士）已发展为敏感和选择性测定7 benzoylphenylurea农药残留（除虫脲， triflumuron ，芬奴隆， flufenoxuron ，伏虫隆， chlorfuazuron ，氟铃脲）在梨婴儿purée ，集中柠檬汁，番茄和纸浆。一般的样本提取/分割方法为我们建立了多重方法已用于。整个程序涉及的提取残留物，用丙酮和分割成乙酸乙酯/环己烷。色谱法测定演出使用C18柱和isocratic洗脱。 14 MS / MS分析过渡的前体离子监测（二为每个农药）使用负面的ESI 。大多数的平均回收率在强化各级0.002-0.020和0.020-0.200毫克/公斤均在范围77-102 ％，相对标准偏差之间的2和10 ％。优秀的敏感性和选择性本的LC / MS / MS法允许的定量和鉴定在低水平，在困难的矩阵与运行时间4分钟。

3.high -高效液相色谱法测定苯甲酰脲类杀虫剂残留的葡萄和葡萄酒使用液体和固相萃取
乔治e. miliadisa ，尼古拉斯g. tsiropoulosb ，和pipina g. aplada - sarlisa
摘要
的含量测定方法的苯甲酰脲类杀虫剂除虫脲， triflumuron ，伏虫隆，芬奴隆和flufenoxuron在葡萄和葡萄酒的高效液相色谱法已开发并验证。葡萄样品（ 50克）匀浆，并用乙酸乙酯提取-硫酸钠和进一步清理行动的固相萃取硅胶吸附剂。葡萄酒样品（ 10毫升）稀释水（ 1:3 ）被固相提取一对十八剂的使用甲醇作为淋洗液。农药分离，一反相十八窄口径柱梯度洗脱和残留的测定紫外二极管阵列检测器。校准样线性范围为0.05-5 μ g / ml的。回收率苯甲酰脲类农药从飙升的葡萄（ 0.02-2.0毫克/千克）和葡萄酒（ 0.01 - 0.2mg /升） 85.8-101.6 ％和69.1-104.8 ％，分别和限制量化为这些杀虫剂< 0.01毫克/公斤，为葡萄和“ < 0.01毫克/升的葡萄酒。该方法用于测定flufenoxuron和伏虫隆残留的葡萄从治疗领域和在生产的葡萄酒。

4 。证监会-紫外分光光度法测定灭幼脲残留量，伏虫隆和triflumuron在苹果和梨浆为婴儿食品
长比基，长巴尔博，甲达马托和澳Panero ）
简要的一种方法，以确定残留农药灭幼脲（德国足协），伏虫隆（专责组）， triflumuron （水杉总黄酮）在0.01 ppm的回收率在60 ％以上，在苹果和梨浆为婴儿食品中描述的。德国足协，专责组和水杉总黄酮提取与甲醇，并清理了固相萃取使用采用C18固定相和甲醇为流动相。分析三个农药是由证监会紫外线波长为254 nm ，使用二醇栏，和CO2在30 MPa和40 ° C时改性乙腈（ 10 ％）为流动相。

补充答案：

液色迷人气质出众回复于2008/05/05

1. 鱼类饲料中双氟苯隆和四氟苯隆的高效液相检测
作者：Victor Hormazabal; Magne Yndestad
摘要：
一种通过HPLC检测鱼类饲料中双氟苯隆和四氟苯隆的简单方法。样品在HPLC上样前，用丙酮-四氢呋喃萃取，并用四氢呋喃洗脱。鱼类饲料中双氟苯隆和四氟苯隆的定量下限分别为0.25和0.4g/kg。

yinhjcom回复于2008/05/05

翻译如下（错误之处，敬请谅解）1。Diflubenzuron和Teflubenzuron的决心在鱼饲料由高性能液相色谱作者：胜者Hormazabal; 为diflubenzuron的决心和teflubenzuron在鱼饲料由HPLC提出Magne Yndestad摘要A简单的方法。样品提取了与丙酮- tetrahydrofurane并且用tetrahydrofurane稀释了，在高性能液体色谱之前。量化低限是0.25和0.4 g/kg。为diflubenzuron和teflubenzuron在鱼哺养，分别。七benzoylphenylurea杀虫药的2.Determination在被处理的水果和蔬菜使用高性能液相色谱或纵排质谱分析安娜Sannino，Mirella Bandini摘要A液体色谱分析的方法以electrospray电离纵排质谱分析(LC/ESI-MS/MS)为七benzoylphenylurea杀虫药残滓被开发了(diflubenzuron、triflumuron、lufenuron、flufenoxuron、teflubenzuron、chlorfuazuron， hexaflumuron)的敏感和有选择性的决心在梨婴孩purée，集中了柠檬汁和蕃茄黏浆状物质。为我们的建立的multiresidue方法使用了一般样品提取或分开方法。整个做法介入残滓的提取与丙酮和分开入乙酸乙酯或环己烷。色谱分析的决心使用C18专栏和isocratic洗提进行了。前体离子的十四MS/MS转折使用消极ESI被监测了(二为每杀虫剂)。多数卑鄙补救在0.002-0.020和0.020-0.200 mg/kg的设防水平是在范围77-102%以相对标准偏差在2和10%之间。这个LC/MS/MS方法优秀敏感性和选择性在困难的矩阵允许测量和证明在低水平以运行时间4 min。 benzoylurea杀虫药残滓的3.High表现液体色谱分析的决心在葡萄和酒使用液体和固体阶段提取乔治E。 Miliadisa， Nicholas G。 Tsiropoulosb，和Pipina G。 Aplada-Sarlisa摘要A方法为benzoylurea杀虫药diflubenzuron、triflumuron、teflubenzuron、lufenuron和flufenoxuron的决心在葡萄和酒由HPLC被开发了并且被确认了。葡萄样品(50 g)在硅土吸着剂均匀了并且提取了与乙基固体阶段提取清洗的醋酸盐钠硫酸盐和更加进一步。用水(10机器语言)稀释的葡萄酒样品(1 ：在octadecyl吸着剂)是固体阶段的提取的3使用甲醇作为洗提液。杀虫剂在一反回阶段octadecyl被分离了由梯度洗脱狭窄使专栏不耐烦，并且残滓确定了与一台紫外二极管列阵探测器。定标剧情是线性的在范围0.05-5 μg/ml。 benzoylurea杀虫剂补救从尖葡萄(0.02-2.0 mg/kg)和酒(0.01-0.2mg/l)分别为85.8-101.6%和69.1-104.8%，和量化极限为这些杀虫药是 <0.01 mg/kg为葡萄和 <0.01 mg/l为酒。方法被运用了于flufenoxuron和teflubenzuron残滓的决心在葡萄从被对待的领域和在被生产的酒。 4. diflubenzuron残滓、teflubenzuron和triflumuron在苹果和梨黏浆状物质的SFC-UV决心为婴儿食品C。 Bicchi， C。 Balbo， A。 D'Amato和O。 Panero确定残滓的总结A方法diflubenzuron (DFB)， teflubenzuron (TFB)， triflumuron (TFM)在0.01 ppm以补救在60%之上在苹果和梨黏浆状物质为婴儿食品被描述。提取与甲醇，并且SPE清扫DFB、TFB和TFM使用C18固定相和甲醇流动相。对三杀虫剂的分析是由SFC-UV在254毫微米使用二醇专栏和二氧化碳在30 MPa和40°C修改以乙腈(10%)流动相。

何当奇回复于2008/05/05

楼主说一篇，可是好像不仅仅是这样的？？

zhuxiugao回复于2008/05/05

呵呵，楼主好像是用翻译器弄得吧。精神可嘉啊