主题：【求助】Bruker AV300 可否也能做DEPTQ和 DOSY？

原文由 aspect 发表:
Bruker AV300 可否也能做DEPTQ和 DOSY？

DEPTQ
;deptq
;avance-version (05/04/19)
;dept polarization transfer
;with decoupling during acquisition
;with variable read pulse
; written by BER, modified and tested by MEB
;R. Burger & P. Bigler, JMR 135, 529 534 (1998)

"p2=p1*2"
"p4=p3*2"
"d2=1s/(cnst2*2)"
"d12=20u"
"p0=(p3/90)*cnst9"
"DELTA=p1*4/3.1416"
1 ze
30m do:f2
d1
d12 pl2:f2
(p1 ph2 d2):f1
(p2 ph3 d2):f1 (p3 ph1):f2
(p1 ph1 d2):f1 (p4 ph3):f2
(p2 ph5 d2):f1 (p0 ph4):f2
DELTA pl12:f2
go=2 ph31 cpd2:f2
30m do:f2 mc #0 to 2 F0(zd)
exit
;pl1 : f1 channel - power level for pulse (default)
;pl2 : f2 channel - power level for pulse (default)
;pl12 : f2 channel - power level for CPD/BB decoupling
;cnst9 : read pulse - 45, 90 or 135
;p0 : f2 channel - 45, 90 or 135 degree high power pulse
; 45 degree - X negative, XH, XH2 and XH3 all positive
; 90 degree - X negative, XH positive
; 135 degree - X, XH2 negative, XH, XH3 positive,
;p1 : f1 channel - 90 degree high power pulse
;p2 : f1 channel - 180 degree high power pulse
;p3 : f2 channel - 90 degree high power pulse
;p4 : f2 channel - 180 degree high power pulse
;d1 : relaxation delay; 1-5 * T1
;d2 : 1/(2 * J(XH))
;d12 : delay for power switching [20 usec]
;cnst2 : = J(XH)
;NS : 4 * n, total number of scans: NS * TD0
;DS : 8

AVANCE 500
AVANCE 500

Multiplicity editing including quaternary carbons improved performance for the 13C-DEPTQ pulse sequence
13C-DEPTQ pulse sequence

只要硬件满足就应该基本可以做了。