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Pesticide | a | b | c | d | e | f | g | h | i | j | k | l | Rec mean | CV [%] mean | Chr | Interface | Detector | ISTD | ISTD addition step | Calibration | Calibration details | Notes |
2,4,5-T-Methylester | 120 | 120 | 110 | 110 | 120 | 116 | 4,7 | GC | EI (pos) | Single Quad. | Triphenylmethane (ISTD) | After add. of solvent | Matrix matched, same matrix |
原文由 辣椒炒肉(yzwujing) 发表:Single Experiment
Experiment No.: Laboratory: Date: Validation context: Internal validation Validation context details: Commodity: Cucumber
Spiking step: Commodity (bef. extraction) Spiking level: 0,01 Extraction method: QuEChERS (citrate) Extraction pH: pH 5-5.5 (Citrate) Cleanup: Dispersive SPE Cleanup details: MgSO4/PSA (150/25 mg/mL) Post cleanup details: pH to ~5 w. formic acid
Pesticide a b c d e f g h i j k l Rec mean CV [%] mean Chr Interface Detector ISTD ISTD addition step Calibration Calibration details Notes 2,4,5-T-Methylester 120 120 110 110 120 116 4,7 GC EI (pos) Single Quad. Triphenylmethane (ISTD) After add. of solvent Matrix matched, same matrix
原文由 MMYG(jl070869) 发表:原文由 辣椒炒肉(yzwujing) 发表:Single Experiment
Experiment No.: Laboratory: Date: Validation context: Internal validation Validation context details: Commodity: Cucumber
Spiking step: Commodity (bef. extraction) Spiking level: 0,01 Extraction method: QuEChERS (citrate) Extraction pH: pH 5-5.5 (Citrate) Cleanup: Dispersive SPE Cleanup details: MgSO4/PSA (150/25 mg/mL) Post cleanup details: pH to ~5 w. formic acid
Pesticide a b c d e f g h i j k l Rec mean CV [%] mean Chr Interface Detector ISTD ISTD addition step Calibration Calibration details Notes 2,4,5-T-Methylester 120 120 110 110 120 116 4,7 GC EI (pos) Single Quad. Triphenylmethane (ISTD) After add. of solvent Matrix matched, same matrix
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