主题：【求助】寻求氟虫腈最大残留量

氟虫腈（fipronil）的残留限量可以参考：  http://www.m5.ws001.squarestart.ne.jp/foundation/agrdtl.php?a_inq=57000

Simple method for the determination of trace levels of pesticides in honeybees using matrix solid-phase dispersion and gas chromatography
Abstract
A simple multiresidue method for the determination of insecticides in honeybees is described. The developed method is based on the matrix solid-phase dispersion technique. A total number of 12 insecticides (azinfos-methyl, buprofezin, chlorpyriphos, chlorpyriphos-methyl, diazinon, ethion, fenitrothion, fipronil, methidathion, phosalone, pirimicarb, propoxur) used on flowering fields are determined by this method. The method uses Florisil and silica as dispersing agents, alumina and silica as cleanup adsorbents and a low polarity solvent system to elute pesticide residues from the honeybee samples. The insecticides were quantified using capillary gas chromatography with a nitrogen–phosphorus detector. The method has shown good recovery (70–110%) for various levels of spiked samples (0.01–1.0 mg/kg). The relative standard deviations were in the range of 2–8% for all pesticides studied. The limits of detection were in the range of 0.005–0.05 mg/kg. The procedure can be applied for the determination of residues of low-polarity and medium polarity pesticides in honeybee samples.

  http://www.sciencedirect.com/science?_ob=ArticleURL&_udi=B6TG8-476TN4R-1&_user=1915929&_rdoc=1&_fmt=&_orig=search&_sort=d&view=c&_version=1&_urlVersion=0&_userid=1915929&md5=27414935989ecbe2dfece7a6275fbd86
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搜索出的结果见图。各个国家（简称）的限量值

原文由 hotdoglet 发表:
氟虫腈（fipronil）的残留限量可以参考：  http://www.m5.ws001.squarestart.ne.jp/foundation/agrdtl.php?a_inq=57000

我们也是用这个网址查的，是厚生省官方网站链接的。

谢谢了，非常有用，请问哪位朋友用气相色谱（FPD检测器的，我这边只有FPD检测器）检测过氟虫腈的残留含量，我这几天一直在用气谱测量它的1PPM标样，响应值一直不高，我都急死了。谢谢朋友给予指点。告诉我检测条件应该如何，响应值才能提高。