TESTS
Nitrates: maximum 0.2 ppm.
Place 5 ml in a test-tube immersed in iced water, add 0.4 ml of a 100 g/l solution of potassium chloride R, 0.1 ml of diphenylamine solution R and, dropwise with shaking, 5 ml of nitrogen-free sulphuric acid R. Transfer the tube to a water-bath at 50 °C. After 15 min, any blue colour in the solution is not more intense than that in a reference solution prepared at the same time in the same manner using a mixture of 4.5 ml of nitrate-free water R and 0.5 ml of nitrate standard solution (2 ppm NO3) R.
硝酸盐:取本品5ml置试管中,于冰浴中冷却,加100g/l氯化钾溶液0.4ml与0.1%二苯胺溶液0.1ml,边摇边滴加无氮的硫酸5ml,摇匀,将试管于50℃水浴中放置15分钟,溶液产生的蓝色与标准硝酸盐溶液(2 ppm NO3)0.5ml,加无硝酸盐的水4.5ml,在同一时间用同一方法处理后的颜色比较,不得更深。
测试
硝酸盐: 最大0.2ppm
于冰浴中冷却....浸入冰浴中 即可
无氮硫酸
其它基本无异议