获得0积分，您同时完成了每日任务，有额外的积分奖励，请前往APP领取
立即前往
| Column色谱柱： | Waters BEH C18 (2.1×100 mm，1.7 μm) |
| Column oven柱温： | 45 °C |
| Flow rate流速： | 0.40 mL/min |
| Injection volume | 5 μL |
| 进样量： | |
| Sample temperature | 10 °C |
| 样品盘温度： |
| No | Time | Rate | %A | %D | Curve |
| (min) | (mL/min) | (5 mmol/L 甲酸铵溶液%) | (乙腈) | ||
| 1 | Initial | 0.4 | 90 | 10 | Initial |
| 2 | 0.75 | 0.4 | 90 | 10 | 6 |
| 3 | 5.3 | 0.4 | 45 | 55 | 6 |
| 4 | 5.31 | 0.4 | 5 | 95 | 6 |
| 5 | 5.8 | 0.48 | 5 | 95 | 6 |
| 6 | 6.5 | 0.5 | 90 | 10 | 1 |
| 7 | 6.51 | 0.4 | 90 | 10 | 1 |
| 8 | 7 | 0.4 | 90 | 10 | 1 |
| Compound Name | Parent(m/z) | Daughter(m/z) | Dwell(s) | Cone(V) | Collision(V) | RT(min) |
| AMPA | 334 | 112* | 0.029 | 20 | 10 | 4.92 |
| AMPA | 334 | 156 | 0.029 | 20 | 10 | 4.92 |
| glyphosate | 392 | 88* | 0.029 | 20 | 15 | 3.94 |
| glyphosate | 392 | 214 | 0.029 | 20 | 10 | 3.94 |
| glyphosate-d | 395 | 91 | 0.029 | 25 | 15 | 3.95 |
| Glufosinate Ammonium | 404 | 136* | 0.029 | 30 | 15 | 4.31 |
| Glufosinate Ammonium | 404 | 208.02 | 0.029 | 30 | 10 | 4.31 |
| Glufosinate Ammonium-d3 | 407 | 139 | 0.025 | 30 | 15 | 4.32 |
原文由 Insm_fe8f17c4(Insm_fe8f17c4) 发表:仪器为TQS-micro Column色谱柱：Waters BEH C18 (2.1×100 mm，1.7 μm)Column oven柱温：45 °CFlow rate流速：0.40 mL/minInjection volume5 μL进样量：Sample temperature10 °C样品盘温度： NoTimeRate%A%DCurve(min)(mL/min)(5 mmol/L 甲酸铵溶液%)(乙腈)1Initial0.49010Initial20.750.49010635.30.44555645.310.4595655.80.48595666.50.59010176.510.490101870.490101 Compound NameParent(m/z)Daughter(m/z)Dwell(s)Cone(V)Collision(V)RT(min)AMPA334112*0.02920104.92AMPA3341560.02920104.92glyphosate39288*0.02920153.94glyphosate3922140.02920103.94glyphosate-d395910.02925153.95Glufosinate Ammonium404136*0.02930154.31Glufosinate Ammonium404208.020.02930104.31Glufosinate Ammonium-d34071390.02530154.32好的，感恩，我又开始研究了
我的社区
签到
9月发帖享好礼，送拍立得、京东卡
国农验证-重金属能力验证经验分享
SEC技术挑战赛·江湖英雄帖
第三届微课大赛投票进行中ing
