主题:【讨论】关于马尔文粒度分布粒镜片生锈的解决方法

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龙在天
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镜片在用一段时间后,无故的生锈了,想了很多办法都没去掉,请大家帮下忙,你们平时是如何处理的
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修身养性
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镜片是什么材料的呀?

一般是金属或者树脂的
怎么会生锈呢?

原文由 zhengzilong 发表:
镜片在用一段时间后,无故的生锈了,想了很多办法都没去掉,请大家帮下忙,你们平时是如何处理的
litsas
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超声一下试试,超声强度不要太大,超声的时候镜片用东西包一下,以免超声的时候划伤。
kwbing008
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原文由 litsas 发表:
超声一下试试,超声强度不要太大,超声的时候镜片用东西包一下,以免超声的时候划伤。


生锈?没见过。。。又不是铁做的。。。光学元件都不超声的。。超声会破坏表面
jacoblin
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原文由 zhengzilong 发表:
镜片在用一段时间后,无故的生锈了,想了很多办法都没去掉,请大家帮下忙,你们平时是如何处理的


水中的铁锈?肯定是做完样品不及时清洁吧,呵呵。
可以考虑用镜头纸蘸无水酒精用力擦拭看看,或者超声水浴也是可以试试的。眼镜店不是有免费超声清洁镜片嘛,加点洗涤液超声水浴可能有效果。

另外,不行的话小心用稀盐酸溶液擦拭该面,应该没问题,可以试试。
mlb2003
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我们经常测试金属粉末,也有同样的问题(正如专家所说的,操作人员有时偷懒,没有及时清洗!)因为用无水乙醇擦不掉,所以也想用稀释的盐酸或醋酸浸泡一下,但是没有试过,不知道行不行!
在马尔文操作手册上第十章是这样介绍的:
Cleaning the optics
The cell area contains several delicate optical devices that require special cleaning procedures. These devices are:
Protection window
Backscatter detectors
Lens
Dust on the surfaces of the devices can be removed using a compressed gas duster can. Keep the can upright while in use to prevent liquid emerging. Alternatively use a specialist camera lens brush. If a brush is used avoid handling the bristles as grease from fingers will be transferred to the optics. If the cleanliness of the brush is in doubt, rinse it in ethanol and let it dry before using it.
Caution!
Do not wipe the devices with an ordinary dry cloth as this will cause scratches. Always use the procedure below to clean the surfaces.
Inspect the devices by reflected light and see if there are any smears or prints on them. If so then you must wipe their surfaces using the following guidelines.
Breathe on the surface of the device to wet it.
Use a good quality lens tissue and gently wipe it over the wetted surface once. Do not put your fingers on the device during this wipe. re-inspect and if still marked, then repeat with another clean tissue.
If this does not eliminate the mark, then consider the use of a liquid cleaner such as Ethanol Absolute or Propan-2-ol. This can be soaked on a cotton wool bud and wiped across the device gently. Use one pass over the device and then discard to avoid scratching. Re-inspect and repeat until clean.
All optical devices outlined above should be inspected for cleanliness every day.
清洗光学元件:
样品池区包含有一些精密的光学元件,要求特殊清洗程序,这些部件是:
保护窗;
背散射检测器;
透镜;
元件表面的灰尘可用压缩气除尘器清除,应保持除尘器是竖直的,防止液体外流,也可以使用专业的相机清理刷,如用此刷要避免手拿着刷毛,因为手指的油脂物会传送的光学元件上,如果弄不清刷子是否清洁,可在乙醛中漂洗,但用前要晾干;
注意:
不要用普通的干布来擦洗元件,这会导致划伤,用下列的程序来清洗表面;
通过反射光来观察元件是否有油渍或印迹,如果有遵循下面指导来擦洗;
对着元件表面呵气使它潮湿;
使用质量好的镜头纸,一次性轻轻地在湿面上擦拭,在擦拭过程中,不要将手指放在设备上,如观察还有污点,用另一张干净镜头纸在擦一次;
如果这样仍不能消除污点,考虑用液体清洁液如Ethanol Absolute 或 Propan-2-ol来清理。将柔软地羊毛制品浸透清洁液,然后轻轻地擦拭,只擦一次避免划痕,再观察并重复直到清洁;
每天都应该对以上所提到地光学元件进行清洁度检查;

只是不知道 Propan-2-ol是什么“东东”!
jacoblin
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原文由 mlb2003 发表:
我们经常测试金属粉末,也有同样的问题(正如专家所说的,操作人员有时偷懒,没有及时清洗!)因为用无水乙醇擦不掉,所以也想用稀释的盐酸或醋酸浸泡一下,但是没有试过,不知道行不行!
在马尔文操作手册上第十章是这样介绍的:
Cleaning the optics
The cell area contains several delicate optical devices that require special cleaning procedures. These devices are:
Protection window
Backscatter detectors
Lens
Dust on the surfaces of the devices can be removed using a compressed gas duster can. Keep the can upright while in use to prevent liquid emerging. Alternatively use a specialist camera lens brush. If a brush is used avoid handling the bristles as grease from fingers will be transferred to the optics. If the cleanliness of the brush is in doubt, rinse it in ethanol and let it dry before using it.
Caution!
Do not wipe the devices with an ordinary dry cloth as this will cause scratches. Always use the procedure below to clean the surfaces.
Inspect the devices by reflected light and see if there are any smears or prints on them. If so then you must wipe their surfaces using the following guidelines.
Breathe on the surface of the device to wet it.
Use a good quality lens tissue and gently wipe it over the wetted surface once. Do not put your fingers on the device during this wipe. re-inspect and if still marked, then repeat with another clean tissue.
If this does not eliminate the mark, then consider the use of a liquid cleaner such as Ethanol Absolute or Propan-2-ol. This can be soaked on a cotton wool bud and wiped across the device gently. Use one pass over the device and then discard to avoid scratching. Re-inspect and repeat until clean.
All optical devices outlined above should be inspected for cleanliness every day.
清洗光学元件:
样品池区包含有一些精密的光学元件,要求特殊清洗程序,这些部件是:
保护窗;
背散射检测器;
透镜;
元件表面的灰尘可用压缩气除尘器清除,应保持除尘器是竖直的,防止液体外流,也可以使用专业的相机清理刷,如用此刷要避免手拿着刷毛,因为手指的油脂物会传送的光学元件上,如果弄不清刷子是否清洁,可在乙醛中漂洗,但用前要晾干;
注意:
不要用普通的干布来擦洗元件,这会导致划伤,用下列的程序来清洗表面;
通过反射光来观察元件是否有油渍或印迹,如果有遵循下面指导来擦洗;
对着元件表面呵气使它潮湿;
使用质量好的镜头纸,一次性轻轻地在湿面上擦拭,在擦拭过程中,不要将手指放在设备上,如观察还有污点,用另一张干净镜头纸在擦一次;
如果这样仍不能消除污点,考虑用液体清洁液如Ethanol Absolute 或 Propan-2-ol来清理。将柔软地羊毛制品浸透清洁液,然后轻轻地擦拭,只擦一次避免划痕,再观察并重复直到清洁;
每天都应该对以上所提到地光学元件进行清洁度检查;

只是不知道 Propan-2-ol是什么“东东”!


问了学化学的专家,Propan-2-ol是异丙醇。
mlb2003
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恶狼
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注意你平时做样品时用的什么水,可能水自来水没有处理好,很容易生锈的,用纸擦擦就好了,以后注意一下自己的测试样品时的水质。没什么好的办法
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