主题:【第六届原创】ICP-OES同时测定硅酸盐中氧化物的含量分析

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国家标准方法GB/T14506-2010硅酸盐岩石化学分析方法,主要是采用重量法和滴定法来分析氧化物和金属含量,方法耗时很多,效率极其低下,有时候一个样品全部做下来可能要10天半月的,大家有没有想过用ICP-OES来一次分析呢?也许有人会说没有可能,那就让事实来说话吧,事实属于雄辩。

Number

Analytes

Units

Detection  Limit

Upper  Limits

1

Al2O3

%

0.01

100

2

BaO

%

0.01

100

3

CaO

%

0.01

100

4

Cr2O3

%

0.01

100

5

Fe2O3

%

0.01

100

6

K2O

%

0.01

100

7

MgO

%

0.01

100

8

MnO

%

0.01

100

9

Na2O

%

0.01

100

10

P2O5

%

0.01

100

11

SiO2

%

0.01

100

12

SrO

%

0.01

100

13

TiO2

%

0.01

100

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Al2O3

CRM ID

Obs.

Lower

Nom.

Upper

% Rec.

P/F

Blank 1

BLANK

0.000

NA

NA

NA

NA

NA

1

G2000

9.57

9.02

9.5

9.99

100.7%

PASS

2

G2000

9.46

9.02

9.5

9.99

99.6%

PASS

3

OREAS-13P

18.95

18.25

19.2

20.2

98.7%

PASS

4

OREAS-13P

19.35

18.25

19.2

20.2

100.8%

PASS

5

OREAS-45P

12.7

12.22

12.89

13.55

98.5%

PASS

6

OREAS-45P

12.75

12.22

12.89

13.55

98.9%

PASS

7

OGGeo08

13.6

12.72

13.41

14.10

101.4%

PASS

8

OGGeo08

13.55

12.72

13.41

14.10

101.0%

PASS

9

MRGeo08

15.4

14.25

15.02

15.79

102.5%

PASS

10

MRGeo08

15.2

14.25

15.02

15.79

101.2%

PASS



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BaO

CRM ID

Obs.

Lower

Nom.

Upper

% Rec.

P/F

Blank 1

BLANK

0.000

NA

NA

NA

NA

NA

1

G2000

0.28

0.24

0.26

0.28

107.7%

PASS

2

G2000

0.28

0.24

0.26

0.28

107.7%

PASS

3

OREAS-13P

0.03

0.01

0.03

0.05

100.0%

PASS

4

OREAS-13P

0.03

0.01

0.03

0.05

100.0%

PASS

5

OREAS-45P

0.03

0.01

0.03

0.05

95.6%

PASS

6

OREAS-45P

0.03

0.01

0.03

0.05

95.6%

PASS

7

OGGeo08

0.11

0.08

0.11

0.13

101.2%

PASS

8

OGGeo08

0.11

0.08

0.11

0.13

101.2%

PASS

9

MRGeo08

0.13

0.10

0.12

0.15

106.0%

PASS

10

MRGeo08

0.12

0.10

0.12

0.15

97.9%

PASS

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CaO 回收率

CRM #

CRM ID

Obs.

Lower

Nom.

Upper

% Rec.

P/F

Blank 1

BLANK

0.000

NA

NA

NA

NA

NA

1

G2000

0.86

0.77

0.82

0.87

104.9%

PASS

2

G2000

0.83

0.77

0.82

0.87

101.2%

PASS

3

OREAS-13P

9.35

9.12

9.61

10.1

97.3%

PASS

4

OREAS-13P

9.68

9.12

9.61

10.1

100.7%

PASS

5

OREAS-45P

0.4

0.38

0.42

0.46

95.3%

PASS

6

OREAS-45P

0.43

0.38

0.42

0.46

102.4%

PASS

7

OGGeo08

3.06

2.98

3.15

3.33

97.0%

PASS

8

OGGeo08

3.04

2.98

3.15

3.33

96.4%

PASS

9

MRGeo08

3.73

3.59

3.80

4.01

98.2%

PASS

10

MRGeo08

3.67

3.59

3.80

4.01

96.6%

PASS

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Cr2O3回收率

CRM #

CRM ID

Obs.

Lower

Nom.

Upper

% Rec.

P/F

Blank 1

BLANK

0.000

NA

NA

NA

NA

NA

1

G2000

0.02

<0.01

0.02

0.03

100.0%

PASS

2

G2000

0.02

<0.01

0.02

0.03

100.0%

PASS

3

OREAS-13P

0.02

<0.01

0.02

0.03

100.0%

PASS

4

OREAS-13P

0.02

<0.01

0.02

0.03

100.0%

PASS

5

OREAS-45P

0.16

0.14

0.17

0.20

94.1%

PASS

6

OREAS-45P

0.16

0.14

0.17

0.20

94.1%

PASS

7

OGGeo08

0.01

<0.01

0.01

0.03

100.0%

PASS

8

OGGeo08

0.01

<0.01

0.01

0.03

100.0%

PASS

9

MRGeo08

0.01

<0.01

0.02

0.04

50.0%

PASS

10

MRGeo08

0.02

<0.01

0.02

0.04

100.0%

PASS



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Fe2O3回收率

CRM #

CRM ID

Obs.

Lower

Nom.

Upper

% Rec.

P/F

Blank 1

BLANK

0.000

NA

NA

NA

NA

NA

1

G2000

5.54

5.15

5.43

5.71

102.0%

PASS

2

G2000

5.49

5.15

5.43

5.71

101.1%

PASS

3

OREAS-13P

10.35

10.3

10.85

11.4

95.4%

PASS

4

OREAS-13P

10.7

10.3

10.85

11.4

98.6%

PASS

5

OREAS-45P

26.5

26.09

27.48

28.87

96.4%

PASS

6

OREAS-45P

26.7

26.09

27.48

28.87

97.2%

PASS

7

OGGeo08

7.84

7.62

8.04

8.46

97.5%

PASS

8

OGGeo08

7.78

7.62

8.04

8.46

96.8%

PASS

9

MRGeo08

5.78

5.59

5.91

6.22

97.9%

PASS

10

MRGeo08

5.66

5.59

5.91

6.22

95.8%

PASS

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K2O回收率

CRM #

CRM ID

Obs.

Lower

Nom.

Upper

% Rec.

P/F

Blank 1

BLANK

0.000

NA

NA

NA

NA

NA

1

G2000

1.58

1.47

1.56

1.65

101.3%

PASS

2

G2000

1.58

1.47

1.56

1.65

101.3%

PASS

3

OREAS-13P

0.55

0.52

0.55

0.59

100.0%

PASS

4

OREAS-13P

0.55

0.52

0.55

0.59

100.0%

PASS

5

OREAS-45P

0.4

0.38

0.42

0.46

94.9%

PASS

6

OREAS-45P

0.4

0.38

0.42

0.46

94.9%

PASS

7

OGGeo08

3.49

3.48

3.68

3.89

94.7%

PASS

8

OGGeo08

3.53

3.48

3.68

3.89

95.8%

PASS

9

MRGeo08

3.77

3.68

3.89

4.11

96.8%

PASS

10

MRGeo08

3.71

3.68

3.89

4.11

95.3%

PASS

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MgO回收率

CRM #

CRM ID

Obs.

Lower

Nom.

Upper

% Rec.

P/F

Blank 1

BLANK

0.000

NA

NA

NA

NA

NA

1

G2000

1.28

1.19

1.26

1.33

101.6%

PASS

2

G2000

1.26

1.19

1.26

1.33

100.0%

PASS

3

OREAS-13P

5.28

5.16

5.44

5.72

97.1%

PASS

4

OREAS-13P

5.43

5.16

5.44

5.72

99.8%

PASS

5

OREAS-45P

0.34

0.33

0.36

0.40

93.2%

PASS

6

OREAS-45P

0.34

0.33

0.36

0.40

93.2%

PASS

7

OGGeo08

2.15

2.11

2.24

2.38

95.8%

PASS

8

OGGeo08

2.15

2.11

2.24

2.38

95.8%

PASS

9

MRGeo08

2.35

2.23

2.37

2.51

99.2%

PASS

10

MRGeo08

2.3

2.23

2.37

2.51

97.1%

PASS

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MnO的回收率

CRM #

CRM ID

Obs.

Lower

Nom.

Upper

% Rec.

P/F

Blank 1

BLANK

0.000

NA

NA

NA

NA

NA

1

G2000

0.08

0.07

0.08

0.09

100.0%

PASS

2

G2000

0.07

0.07

0.08

0.09

87.5%

PASS

3

OREAS-13P

0.14

0.13

0.15

0.16

93.3%

PASS

4

OREAS-13P

0.15

0.13

0.15

0.16

100.0%

PASS

5

OREAS-45P

0.16

0.14

0.16

0.19

97.6%

PASS

6

OREAS-45P

0.17

0.14

0.16

0.19

103.7%

PASS

7

OGGeo08

0.07

0.05

0.07

0.09

101.1%

PASS

8

OGGeo08

0.07

0.05

0.07

0.09

101.1%

PASS

9

MRGeo08

0.08

0.05

0.08

0.10

105.2%

PASS

10

MRGeo08

0.08

0.05

0.08

0.10

105.2%

PASS

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Na2O的回收率

CRM #

CRM ID

Obs.

Lower

Nom.

Upper

% Rec.

P/F

Blank 1

BLANK

0.000

NA

NA

NA

NA

NA

1

G2000

0.21

0.2

0.22

0.24

95.5%

PASS

2

G2000

0.21

0.2

0.22

0.24

95.5%

PASS

3

OREAS-13P

2.6

2.41

2.55

2.69

102.0%

PASS

4

OREAS-13P

2.65

2.41

2.55

2.69

103.9%

PASS

5

OREAS-45P

0.12

0.08

0.11

0.13

109.9%

PASS

6

OREAS-45P

0.12

0.08

0.11

0.13

109.9%

PASS

7

OGGeo08

2.6

2.39

2.54

2.69

102.4%

PASS

8

OGGeo08

2.55

2.39

2.54

2.69

100.4%

PASS

9

MRGeo08

2.85

2.56

2.72

2.87

104.9%

PASS

10

MRGeo08

2.81

2.56

2.72

2.87

103.4%

PASS



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P2O5的回收率

CRM #

CRM ID

Obs.

Lower

Nom.

Upper

% Rec.

P/F

Blank 1

BLANK

0.000

NA

NA

NA

NA

NA

1

G2000

0.22

0.2

0.22

0.24

100.0%

PASS

2

G2000

0.22

0.2

0.22

0.24

100.0%

PASS

3

OREAS-13P

0.16

0.15

0.17

0.19

94.1%

PASS

4

OREAS-13P

0.17

0.15

0.17

0.19

100.0%

PASS

5

OREAS-45P

0.1

0.08

0.11

0.13

92.8%

PASS

6

OREAS-45P

0.1

0.08

0.11

0.13

92.8%

PASS

7

OGGeo08

0.18

0.17

0.20

0.23

90.2%

PASS

8

OGGeo08

0.18

0.17

0.20

0.23

90.2%

PASS

9

MRGeo08

0.24

0.21

0.24

0.28

98.2%

PASS

10

MRGeo08

0.23

0.21

0.24

0.28

94.2%

PASS

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